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For general references on chiral Ti complexes and their utility in catalysis see: (a) Duthaler, R. O.; Hafner, A. Chem. Rev. 1992, 92, 807-832.
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16
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85088002454
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1H NMR spectroscopy.
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17
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3743104830
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note
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3.
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18
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3743091505
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San Francisco, CA; American Chemical Society: Washington DC, INOR 208
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For the first evidence of this type of interaction in early-metal complexes, see: Walsh, P. J.; Gantzel, P., Pritchett, S.; Ho, D. Abstracts of Papers, 213th National Meeting of the American Chemical Society, San Francisco, CA; American Chemical Society: Washington DC, 1997; INOR 208.
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Walsh, P.J.1
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Pritchett, S.; Gantzel, P.; Walsh, P. J. Organometallics 1997, 16, 5130-5132.
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0003437226
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Ellis Horwood: Chichester, U.K., Chapter 8
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17c (a) Encyclopedia of Organic Reagents; Paquette, L. A., Ed.; Wiley: Chichester, U.K., 1995; Vol. 3, pp 1732-1733. (b) Renzinger, E.; Kornicker, W. Chem. Ber., 1961, 2263-2267. (c) Reactivity observed when ArOH is 2,6-dimethylphenol.
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Paquette, L.A.1
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Renzinger, E.1
Kornicker, W.2
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30
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33845377928
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2. For another synthetic route to 7, see: Durfee, L. D.; Latesky, S. L.; Rothwell, I. P.; Huffman, J. C.; Folting, K. Inorg. Chem. 1985, 24, 4569-4573.
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4 see: Bradley, D. C.; Thomas, I. M. J. Chem. Soc. 1960, 3857-3861. For the synthesis of bis(triflamide) 1c, see: Pikul, S.; Corey, E. J. Org. Synth. 1992, 71, 30-37.
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Pikul, S.1
Corey, E.J.2
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34
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85088002942
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note
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2/hexanes.
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