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note
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2 appear at δ 3.9 and 4.9 ppm. See ref 3 for more discussion.
-
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31
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85087248142
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note
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6, presented in ref 3, reveal such spectral change more clearly.
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32
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3843142411
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note
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The frequency interval between 1a and 1d at -45 °C is practically the same as that at -55 °C and, therefore, is taken as the limiting value.
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