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85034201615
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note
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The peak of benzene (solvent) was observed at 5 min. We tried to separate the side products, which were observed as small peaks. However, we failed to identify the compounds, as the amount of these products were negligible after the separation of recycle-type HPLC.
-
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27
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85034174800
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note
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w = 0.099 for 3337 reflections.
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