Protonation and Alkylation of a Dinuclear Nickel Thiolate Complex

Inorganic Chemistry

Volumn 37, Issue 17, 1998, Pages 4166-4167

  Allan, Christian B ^a,b   Davidson, Gerard ^a   Choudhury, Suranjan B ^a   Gu, Zhijie ^a   Bose, Kurethara ^a   Day, Roberta O ^a   Maroney, Michael J ^a  

^a UNIVERSITY OF MASSACHUSETTS   (United States)

^b NATIONAL HEART LUNG AND BLOOD INSTITUTE   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001599217     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic9804465     Document Type: Article

References (22)

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13. 6: C, 21.38; H, 4.12; N, 4.98. Found: C, 20.87; H, 3.93; N, 4.71.
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15. -1 and backtransform limits of r = 1.1-2.6 Å (uncorrectcd for phase shifts), as described previously (see ref 18). Analysis results are given in the Supporting Information.
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20. 2 employed all of the data and led to a final R = 4.0% for 3220 observed reflections.
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22. 2 solution. The standard three-electrode cell consisted of a glassy carbon working electrode, a Ag wire pseudo reference electrode, and a Pt auxiliary electrode. Potentials were calibrated to the ferrocene/ferrocenium couple and converted to the NHE reference by setting the potential of this couple to +400 mV vs NHE. The values reported were obtained using a 250 mV/s sweep rate.