A stereoselective approach to optically active bifunctional 1,3-dimethyl-1,3-diphenyldisiloxanes

Organic Letters

Volumn 1, Issue 4, 1999, Pages 549-551

  Oishi, Motoi ^a   Kawakami, Yusuke ^a  

^a JAPAN ADVANCED INSTITUTE OF SCIENCE AND TECHNOLOGY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001594362     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol990068n     Document Type: Article

References (24)

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2. (b) Mori, A.; Sato, H.; Mizuno, K.; Hiyama, T.; Shintani, K.; Kawakami, Y. Chem Lett. 1996, 517.
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6. (d) Kawakami, Y.; Kishimoto, N.; Takeshita, K.; Watanabe, T. Design Monom. Polym. 1999, 2, 93.
7. (a) Kawakami, Y.; Ito, Y.; Toida, K. Macromoleclues 1993, 26, 1177.
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12. (b) Li, Y.; Kawakami, Y. Macromolecules 1999, 32, 548.
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16. Since (S)-methyl(1-naphthyl)phenylchlorosilane 1 is unstable to the moisture, the ee was determined on (A)-methyl(1-naphthyl)phenylsilane after the reduction of (S)-1.
17. Sommer, L. H.; Frye, C. L.; Parker, G. A. J. Am. Chem. Soc. 1964, 86, 3276
18. HPLC analysis: Daicel Chem. Ind., CHIRALCEL OD, n-hexane as an eluent, 0.4 mL/min, 254 nm.
19. Kawakami, Y.; Takahashi, T.; Yada, Y.; Imae, I. Polym. J. 1998, 30, 1001.
20. Sommer, L. H.; Michael, K. W.; Korte, W. D. J. Am. Chem. Soc. 1967, 89, 868.
21. Earbon, C.; Steward, O. W. Proc. Chem. Soc. 1963, 59.
22. 1H NMR.
23. +).
24. +).