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4), Air Products and Chemicals, Inc.; N-fluoropyridinium pyridine heptafluorodiborate (Accufluor, NFPy), N-fluorobenzenesulfoniimde (Accufluor, NFSi), N-fluoro-N′-hydroxy-1,4-diazoniabicyclo[2.2.2]octane bis(tetrafluoroborate) (Accufluor, NFTh), Allied Signal Inc.
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1542609630
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note
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3CN (1 L × 2) to give 1278 g (87%) of pure 1b. The crystals were dried at 50°C for 5 h under reduced pressure.
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