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Tetrahedron Letters

Volumn 30, Issue 40, 1989, Pages 5393-5396

Palladium-catalyzed phosphorylation of alkenyl triflates

(2) Holt, Dennis A a Erb, Jill M a

a Department of Medicinal Chemistry Smith Kline and French Laboratories ^* (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001582686 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(01)80576-1 Document Type: Article

Times cited : (87)

References (22)

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9
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10
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- A regioselective entry to vinyl lithiums from unsymmetrical ketones via enol triflates
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- Wulff¹ Peterson² Bauta³ Chan⁴ Faron⁵ Gilbertson⁶ Kaesler⁷ Yang⁸ Murray⁹

11
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12
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15
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- Int. Ed. Engl.
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17
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- A method for the regiospecific synthesis of enol triflates by enolate trapping
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18
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- Commercially available (Aldrich) 50% aqueous hypophosphorous acid was distilled at 38 mmHg, 30–35° C. The distillate solidified upon cooling to −20° C and thereafter was handled as a hygroscopic solid using ordinary precautions to exclude moisture. See also
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19
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- Palladium catalysed alkoxycarbonylation of phenols to benzoate esters
- Bidentate phosphine ligands have been reported to accelerate aryl triflate-palladium-catalyzed carbonylation reactions, however no rate enhancement was observed for the phosphorylations of alkenyl triflates. See, and references cited therein
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- Dolle¹ Schmidt² Kruse³

20
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- 11. We find that our phosphorylation protocol also allows for the preparation of aryl phosphonates and, additionally, aryl phosphinates from aryl triflates provided that one mole-equivalent per palladium of 1,3-bis(diphenylphosphino)propane is added and the reaction temperature is held at 90° C for 4–5 hours.

21
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- (1987) J. Am. Chem. Soc. , vol.109 , pp. 2831
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22
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- Lu¹ Zhu²

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.