Synthetic control over the production of multicomponent sol-gel materials: Fabrication of homogeneous vanadia-silica xerogels with high vanadium content

Chemistry of Materials

Volumn 11, Issue 4, 1999, Pages 1120-1127

  Curran, Matthew D ^a   Gedris, Thomas E ^a   Stiegman, A E ^a   Plett, Gary A ^b  

^a FLORIDA STATE UNIVERSITY   (United States)

^b CALIFORNIA INSTITUTE OF TECHNOLOGY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001572652     PISSN: 08974756     EISSN: None     Source Type: Journal    
DOI: 10.1021/cm981119y     Document Type: Article

References (34)

1. (a) Ulrich, D. R. J. Non-Cryst. Solids 1988, 100, 174.
2. (b) Mackenzie, J. D. J. Non-Cryst. Solids 1988, 100, 162.
3. (a) Kundu, D.; Biswas, P. K.; Ganguli, G. J. Non-Cryst. Solids 1989, 110
4. (b) Dave, B. C.; Dunn, B.; Valentine, J. S.; Zink, J. I. Anal. Chem. 1994, 66, 1120.
5. (c) Badini, G. E.; Grattan, K. T. V.; Tseung, A. C. C. Rev. Sci. Instrum. 1995, 66, 4034.
6. (d) Ghosh, A.; Chakravorty, D. Appl. Phys. Lett. 1991, 59, 855
7. (e) McCulloch, S.; Stewart, R. M.; Guppy, R. M.; Norris, J. O. W. Int. J. Optoelec. 1994, 9, 235.
8. Stiegman, A. E.; Eckert, H.; Plett, G.; Kim, S.-S.; Mark Anderson, M.; Yavrouian, A. Chem. Mater. 1993, 11, 1591.
9. Miller, J. B.; Ko, E. I. J. Catal. 1996, 150, 58.
10. Brinker, C. J.; Scherer, G. W. Sol-Gel Science; Academic Press: San Diego, 1990; p 45.
11. Curran, M. D.; Pooré, D. D.; Stiegman, A. E. Chem. Mater. 1998, 10, 3156.
12. Wokaun, A.; Schraml, M.; Baiker, A. J. Catal. 1989, 116, 595.
13. Livage, J.; Henry, M.; Sanchez, C. Prog. Solid St. Chem. 1988, 18, 259.
14. Yoldas, B. J. Non-Cryst. Solids 1980, 38, 81.
15. (a) Baiker, A.; Dollenmeier, P.; Glinski, M.; Reller, A.; Sharma, V. K. J. Catal. 1988, 111, 273.
16. (b) Dutoit, D. C. M.; Schneider, M.; Fabrizioli, P.; Baiker, A. J. Mater. Chem. 1997, 7, 271.
17. Wang, C.-B.; Deo, G.; Wachs, I. E. J. Catal. 1998, 178, 640.
18. (a) Coltrain, B. K.; Melpolder, S. M.; Salva, J. M. In Ultrastructure Processing of Advanced Materials; Uhlmann, D. R., Ulrich, D. R., Eds.; John Wiley: New York, 1992, p 69. (b) Ref 5, p 212.
19. Lever, A. B. P. Inorganic Electronic Spectroscopy; Elsevier: Amsterdam, 1984; p 384.
20. Chasteen, N. D. In Biological Magnetic Resonance; Plenum Press: New York; 1981; Vol. 3, Chapter 2, p 53.
21. Cotton, F. A.; Wilkinson G. Advanced Inorganic Chemistry, 4th ed.; John Wiley & Son: New York, 1980; p 711.
22. (b) Catana, G.; Rao, R. R.; Weckhuysen, B. M.; Van Der Voort, P.; Vansant, E.; Schoonheydt, R. A. J. Phys. Chem. 1998, 102, 8005 and references therein.
23. (a) Orgaz, F.; Rawson, H. J. Non-Cryst. Solids 1986, 82, 57. (b) Ref 5, p 547.
24. Dahmouche, K.; Bovier, C.; Dumas, J.; Serughetti, J.; Mai, C. J. Mater. Sci. 1995, 30, 4149.
25. Doremus, R. H. Glass Science, 2nd ed.; John Wiley & Son: New York, 1994; p 105.
26. max ) 1430 nm) and ESR spectra (g∥= 1.935, g⊥= 1.993, A∥ ) 199 G, and A⊥ 68 G), as being identical to partially reduced pure vanadia gels which had been previously investigated (Babonneau, F.; Barboux, P.; Josien, F. A.; Livage, J. J. Chim. Phys. 1985, 82, 761
27. and Araki, B.; Audiéres, J. P.; Michaud, M.; Livage, J. Bull. Soc. Chim. Fr. 1981, 9-10, 366.). Identical near-IR and ESR were obtained for the heterogeneous green phase that formed under nitric acid catalysis.
28. Enjalbert, R.; Galy, J. Acta Crystallogr. C 1986, 42, 1467.
29. Oyama, T.; Went, G. T.; Lewis, K. B.; Bell, A. T.; Somorjai, G. A. J. Phys. Chem. 1989, 93, 6786.
30. Scraml-Marth, M.; Wokaum, A.; Pohl, M.; Krauss, H.-L. J. Chem. Soc. Faraday Trans. 1991, 87, 2635.
31. (a) Eckert, H.; Wachs, I. E. J. Phys. Chem. 1989, 93, 6796.
32. (b) Das, N.; Eckert, H.; Hu, H.; Wachs, I. E.; Walzer, J. F.; Feher, F. J. J. Phys. Chem. 1993, 97, 8240.
33. Tran, K.; Hanning-Lee, M. A.; Biswas, A.; Stiegman, A. E.; Scott, G. W. J. Am. Chem. Soc. 1995, 117, 2618.
34. Abello, L.; Husson, E.; Repelin, Y.; Lucazeau, G. Spectrochim. Acta 1983, 7, 641.