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0001413313
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(13. Série), For reasons unknown to us, the yield of 3-bromoprop-2-ynol ranged from nearly 0% to 70%
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(a) Chodkiewicz, W. Ann. Chim. 1957, 2 (13. Série), 819. For reasons unknown to us, the yield of 3-bromoprop-2-ynol ranged from nearly 0% to 70%.
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84892590783
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note
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The strategy via dialkynylborates4 is not compatible with the functional groups used in this paper.
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14
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0040835922
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17
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29
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84892566133
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Vereshchagin, L. I.; Buzilova, S. R.; Bol'shedvorskaya, R. L.; Kirillova, L. P. J. Org. Chem. USSR (Engl. Transl.) 1976, 12, 1174.
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0001677885
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37
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84892575018
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note
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1H signals at 2 and 4 ppm get considerably narrower with temperature increase. This observation is explained with the conformational flexibility of the pyrrolidine ring.
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-
-
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38
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84892591407
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note
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13C NMR spectra was usually too low for detection of the Sn satellites of the alkyne signal.
-
-
-
-
39
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84892609944
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note
-
Although 9d could not be obtained as a pure compound, 9 (R = OH) synthesized from 9d in 91% yield was an analytically pure compound.
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