Syntheses and Molecular Structures of Bis(tert-butylamido)cyclodiphosph(III)azane Cage Complexes of Thallium(I) and Indium(II)

Inorganic Chemistry

Volumn 37, Issue 10, 1998, Pages 2496-2499

  Grocholl, Luke ^a   Schranz, Ingo ^a   Stahl, Lothar ^a   Staples, Richard J ^b  

^a UNIVERSITY OF NORTH DAKOTA   (United States)

^b HARVARD UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001503709     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic9716316     Document Type: Article

References (31)

1. (a) Uhl, W.; Layh, M.; Hiller, W. J. Organomet. Chem. 1989, 368, 139.
2. (b) Schumann, H.; Janiak, C.; Pickardt, J.; Boerner, U. Angew. Chem., Int. Ed. Engl. 1987, 26, 789.
3. (c) Rheingold, A. L.; Liable-Sands, L. M.; Trofimenko, S. J. Chem. Soc., Chem. Commun. 1997, 1691.
4. (d) Schumann, H.; Janiak, C.; Khan, M. A.; Zuckerman, J. J. J. Organomet. Chem. 1988, 354, 7.
5. (e) Hellmann, K. W.; Cade, L. H.; Steiner, A.; Stalke, D.; Moeller, F. Angew. Chem., Int. Ed. Engl. 1997, 36, 160.
6. (f) Veith, M.; Spaniol, A.; Poehlmann, J.; Gross, F.; Huch, V. Chem. Ber. 1993, 126, 1413.
7. (g) Li, X. W.; Pennington, W. T.; Robinson, G. H. J. Am. Chem. Soc. 1995, 117, 7578.
8. (h) Henkel, S.; Klinkhammer, K. W.; Schwarz, W. Angew. Chem., Int. Ed. Engl. 1994, 33, 3, 681.
9. (i) Uhl, W.; Graupner, R.; Hiller, W.; Neumayer, M. Angew. Chem., Int. Ed. Engl. 1997, 36, 62.
10. (j) Schluter, R. D.; Cowley, A. H.; Atwood, D. A.; Jones, R. A.; Bond, M. R.; Carrano, C. J. J. Am. Chem, Soc. 1993, 115, 2070.
11. (k) Klinkhammer, K. W.; Henkel, S. J. Organomet. Chem. 1994, 480, 167.
12. (l) Uhl, W. Angew. Chem., Int. Ed. Engl. 1993, 32, 1386.
13. For a detailed discussion of metal-metal interactions in low-valent group 13 compounds, see: Janiak, C.; Hoffmann, R. J. Am. Chem. Soc. 1990, 112, 5924.
14. (3) Bis(amino)cyclodiphosph(III)azanes are a well-known class of inorganic heterocycles whose function as chelating bis(amide) ligands, however, had not previously been explored. For leading references on these molecules, see: (a) Tarassoli, A.; Haltiwanger, R. C.; Norman, A. D. Inorg. Chem. 1982, 21, 2684. (b) Hill, T. G.; Haltiwanger, R. C.; Thompson, M. L.; Katz, S. A.; Norman, A. D. Inorg. Chem. 1994, 33, 1770. Bulloch, G.; Keat, R. J. Chem. Soc., Dalton Trans. 1974, 2010.
15. Bis(amino)cyclodiphosph(III)azanes are a well-known class of inorganic heterocycles whose function as chelating bis(amide) ligands, however, had not previously been explored. For leading references on these molecules, see: (a) Tarassoli, A.; Haltiwanger, R. C.; Norman, A. D. Inorg. Chem. 1982, 21, 2684. (b) Hill, T. G.; Haltiwanger, R. C.; Thompson, M. L.; Katz, S. A.; Norman, A. D. Inorg. Chem. 1994, 33, 1770. Bulloch, G.; Keat, R. J. Chem. Soc., Dalton Trans. 1974, 2010.
16. Bis(amino)cyclodiphosph(III)azanes are a well-known class of inorganic heterocycles whose function as chelating bis(amide) ligands, however, had not previously been explored. For leading references on these molecules, see: (a) Tarassoli, A.; Haltiwanger, R. C.; Norman, A. D. Inorg. Chem. 1982, 21, 2684. (b) Hill, T. G.; Haltiwanger, R. C.; Thompson, M. L.; Katz, S. A.; Norman, A. D. Inorg. Chem. 1994, 33, 1770. (c) Bulloch, G.; Keat, R. J. Chem. Soc., Dalton Trans. 1974, 2010.
17. Schranz, I.; Stahl, L.; Staples, R. J. Inorg. Chem. 1998, 37, 1493.
18. (a) Veith, M.; Goffing, F.; Huch, V. Chem. Ber. 1988, 121, 943.
19. (b) Veith, M.; Goffing, F.; Becker, S.; Huch, V. J. Organomet. Chem 1991, 406, 105.
20. Cyclodiphosph(III)azanes are also called diazadiphosphetidines - a naming system preferred by CAS.
21. SMART V 4.043 Software for the CCD Detector System; Siemens Analytical Instruments Division: Madison, WI, 1995.
22. SAINT V 4.035 Software for the CCD Detector System; Siemens Analytical Instruments Division: Madison, WI, 1995.
23. SADABS program for absorption corrections using the Siemens CCD Detector System, based on: Blessing, R. Acta Crystalloer. 1995, A51, 33.
24. Sheldrick, G. M. SHELXS-90, Program for the Solution of Crystal Structures; University of Göttingen: Göttingen, Germany, 1990.
25. Sheldrick, G. M. SHELXL-97, Program for the Solution of Crystal Structures; University of Göttingen: Göttingen, Germany, 1997.
26. SHELXTL 5.03 (PC Version), Program Library for Structure Solution and Molecular Graphics; Siemens Analytical Instruments Division: Madison, WI, 1995.
27. Wells, A. F. Structural Inorganic Chemistry, 5th ed.; Oxford University Press: New York, 1984.
28. Cotton, F. A.; Wilkinson, G.; Gaus, P. L. Basic Inorganic Chemistry, 3rd ed.; Wiley: New York, 1995.
29. Khan, M. A.; Peppe, C.; Tuck, D. G. Can. J. Chem. 1984, 62, 601.
30. Freeland, B. H.; Hencher, J. L.; Tuck, D. G.; Contreras, J. G. Inorg. Chem. 1976, 15, 2144.
31. Tuck, D. G. Chem. Soc. Rev. 1993, 22, 269.