NMR imaging of elastomers: A review

Rubber Chemistry and Technology

Volumn 70, Issue 3, 1997, Pages 468-518

  Blumler P ^a   Blumich B ^a  

^a RWTH AACHEN UNIVERSITY   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001498726     PISSN: 00359475     EISSN: None     Source Type: Journal    
DOI: 10.5254/1.3538438     Document Type: Review

References (158)

1. V. J. McBrierty and K. J. Packer, "Nuclear Magnetic Resonance in Solid Polymers," Cambridge Press, Cambridge, 1993.
2. R. A. Komoroski, "High Resolution NMR Spectroscopy of Synthetic Polymers in Bulk," VCH Publishers, Deerfield Beach, 1986.
3. J. Koenig, "Spectroscopy of Polymers," American Chemical Society, Washington, D.C., 1992.
4. K. Landfester, C. Boeffel, M. Lambla, and H. W. Spiess, Macromolecules 29, 5972 (1996).
5. S. Spiegel, K. Schmidt-Rohr, C. Boeffel, and H. W. Spiess, Polymer 34, 4566 (1993).
6. P. Jezzard, C. J. Wiggins, T. A. Carpenter, L. D. Hall, P. Jackson, N. J. Clayden, and N. J. Walton, Adv. Mater. 4, 82 (1992).
7. R. A. Komoroski, Anal. Chem. 65, 1068A (1993).
8. J. L. Koenig, Macromol. Symp. 86, 283 (1994).
9. B. Büimich and W. Kuhn, Eds., "Magnetic Resonance Microscopy," VCH Publishers, Weinheim, 1992.
10. P. Mansfield and P. G. Morris, "NMR Imaging in Biomedicine," in "Advances in Magnetic Resonance," J. S. Waugh, Ed., Suppl. 2, Academic Press, New York, 1982.
11. E. Krestel, "Imaging Systems for Medical Diagnosis," Siemens AG, Berlin, 1990.
12. C. L. Partain, R. R. Price, J. A. Patton, M. V. Kulkarni, and A. E. James, Eds., "Magnetic Resonance Imaging," 2nd ed., W. B. Saunders Co., Philadelphia, 1988, 2v.
13. P. T. Callaghan, "Principles of Nuclear Magnetic Resonance Microscopy," Clarendon Press, Oxford, 1991.
14. P. Blümler and B. Blümich, NMR: Basic Princi. Progr. 30, 209 (1994).
15. K. Schmidt-Rohr and H. W. Spieß, "Multidimensional Solid State NMR and Polymers," Academic Press, London, 1994.
16. R. R. Ernst, G. Bodenhausen, and A. Wokaun, "Principles of Nuclear Magnetic Resonance in One and Two Dimensions," Clarendon Press, Oxford, 1987.
17. W. A. Edelstein, J. M. S. Hutchinson, G. Johnson, and T. W. Redpath, Phys. Med. Biol. 25, 751 (1980).
18. P. Blümler and B. Blümich, Magn. Reson. Imag. 10, 779 (1992).
19. A. Haase, M. Brandl, E. Kuchenbrod, and A. Link, J. Magn. Reson. A 105, 230 (1993).
20. W. Dietrich, G. Bergmann, and R. Gerhards, Z. Anal. Chem. 279, 177 (1976).
21. E. D. Ostroff and J. S. Waugh, Phys. Rev. Lett. 16, 1097 (1966).
22. P. Mansfield and D. Ware, Phys. Rev. 188, 318 (1968).
23. R. Campanella, C. Casieri, F. de Luca, B. C. de Simone, and B. Maraviglia in "Physics of NMR spectroscopy in biology and medicine," B. Maraviglia Ed., Elsevier, Amsterdam, 1988.
24. I. M. Ward and D. W. Hadley, "An Introduction to the Mechanical Properties of Solid Polymers," Wiley, New York, 1993.
25. C. Fülber, B. Blümich, K. Unseld, and V. Herrmann, Kautsch. Gummi, Kunstst. 48, 254 (1995).
26. B. Blümich and P. Blümler, Makromol. Chem. 194, 2133 (1993).
27. C. Chang and R. A. Komoroski, Macromolecules 22, 600 (1989).
28. C. Chang and R. A. Komoroski, in "Solid State NMR of Polymers," L. Mathias Ed., Plenum Press, New York, 1991, ch. 23, p. 363.
29. A. G. Webb, P. Jezzard, L. D. Hall, and S. Ng, Polym. Commun. 30, 363 (1989).
30. J. A. Chudek and G. Hunter, J. Mater. Sci. Lett. 11, 222 (1992).
31. W. Kuhn, I. Theis, and E. Koeller, Mat. Res. Soc. Symp. Proc. 217, 33 (1991).
32. S. N. Sarkar and R. A. Komoroski, Macromolecules 25, 1420 (1992).
33. R. A. Komoroski and S. N. Sarkar, Mater. Res. Soc. Symp. Proc. 217, 3 (1991).
34. R. A. Komoroski and S. N. Sarkar, in Ref [9].
35. J. E. Mark and B. Erman, "Rubberlike Elasticity a Molecular Primer," John Wiley & Sons, New York, 1988.
36. S. Kaufman, W. P. Slichter, and D. D. Davis, J. Polym. Sci. A2, 829 (1971).
37. J. P. Cohen-Addad, Phys. Rev. Lett. 33, 940 (1974).
38. J. P. Cohen-Addad and R. Dupeyre, Polymer 24, 400 (1983).
39. V. M. Litvinov and A. A. Zhdanov, Polym. Sci. U.S.S.R. 29, 1133 (1987).
40. G. Simon, B. Götschmann, D. Matzen, and H. Schneider, Polym. Bull. 21, 475 (1989).
41. K. Baumann and W. Gronski, Kautsch. Gummi, Kunstst. 42, 387 (1989).
42. V. M. Litvinov and H. W. Spiess, Macromol. Chem. 193, 1181 (1992).
43. V. J. McBrierty and J. C. Kenny, Kautsch. Gummi, Kunstst. 47, 342 (1994).
44. H. Lüchow and W. Gronski, Kautschuk-Herbst-Kolloquium, Hannover, Germany, Oct. 24-26, 1996.
45. P. Blümler and B. Blümich, Acta Polymer 44, 125 (1993).
46. L. Garrido, J. L. Ackerman, and J. E. Mark, Mater. Res. Soc. Symp. Proc. 171, 65 (1990).
47. L. Garrido, J. E. Mark, C. C. Sun, J. L. Ackerman, and C. Chang, Macromolecules 24, 4067 (1991).
48. L. Garrido, J. L. Ackerman, J. M. Vevea, and J. E. Mark, Polymer 33, 1826 (1992).
49. J. L. Ackerman, L. Garrido, J. R. Moore, B. Pfleiderer, and Y. Wu, in Ref. [9].
50. J. Queslel, J. E. Mark in "Mechanical and Solvent-Swelling Methods for Characterizing Insoluble Polymers," A. R. Cooper Ed., John Wiley & Sons, New York, 1989, ch. 16.
51. S. R. Smith and J. L. Koenig, Macromolecules 24, 3496 (1991).
52. A. G. Webb and L. D. Hall, Polym. Commun. 31, 422 (1990).
53. A. Alfrey, E. F. Gurnee, and W. G. Lloyd, J. Polym. Sci. C12, 249 (1966).
54. M. R. Halse, H. J. Rahman, and J. H. Strange, Physica B 203, 169 (1994).
55. S. P. Cottrell, M. R. Halse, and J. H. Strange, Meas. Sci. Technol. 1, 624 (1990).
56. A. G. Webb and L. D. Hall, Polym. Commun. 31, 425 (1990).
57. R. S. Clough and J. L. Koenig, J. Polym. Sci. C27, 451 (1989).
58. M. R. Krejsa and J. L. Koenig, RUBBER CHEM. TECHNOL. 64, 635 (1991).
59. M. A. Rana and J. L. Koenig, Macromolecules 27, 3727 (1994).
60. Y. Shen, L. Fei, and X. Zhao, Appl. Magn. Reson. 8, 181 (1995).
61. R. A. Kinsey, RUBBER CHEM. TECHNOL. 63, 407 (1990).
62. J. Schaefer, Macromolecules 5, 427 (1972).
63. J. Schaefer, Macromolecules 6, 882 (1973).
64. M. Andreis and J. L. Koenig, Polym. Prepr. Am. Chem. Soc., Div. Polym. Chem. 29, 29 (1988).
65. W. Gronski, H. Hasenhindl, B. Freund, and S. Wolff, Kautsch. Gummi, Kunstst. 44, 119 (1991).
66. D. E. Demco, S. Hafner, C. Fülber, R. Graf, and H. W. Spiess, J. Chem. Phys. 105, 11285 (1996).
67. G. Simon and H. Schneider, Makromol. Chem., Macromol. Symp. 52, 233 (1991).
68. H. W. Spiess, Angew. Makromol. Chem. 203, 331 (1992).
69. C. Fülber, D. E. Demco, O. Weintraub, and B. Blümich, Macromol. Chem. Phys. 197, 581 (1996).
70. T. J. Rowland and L. C. Labun, Macromolecules 11, 466 (1978).
71. G. C. Munie and J. Jonas, J. Polym. Sci. 18, 1061 (1980).
72. G. Simon, A. Birnstiel, and K.-H. Schimmel, Polym. Bull. 21, 235 (1989).
73. G. Simon, K. Baumann, and W. Gronski, Macromolecules 25, 3624 (1992).
74. P. Sotta, C. Fülber, D. E. Demco, B. Blümich, and H. W. Spiess, Macromolecules 29, 6222 (1996).
75. J. J. Gotlib, M. J. Lifshitz, V. A. Shevelev, I. C. Lishansky, and I. V. Balanina, Vysokomol. Soed. A18, 2299 (1976).
76. V. D. Fedotov, V. M. Thernov, T. N. Khasanovitsh,. Vysokomol. Soed. A20, 919 (1978).
77. V. D. Fedotov and H. Schneider, "Structure and Dynamics of Bulk Polymers by NMR-Methods," (NMR Basic Principles and Progress, v. 21), Springer, Berlin, 1989.
78. W. Gronski, U. Hoffmann, G. Simon, A. Wutzler, and E. R. Straube, RUBBER CHEM. TECHNOL. 65, 63 (1992).
79. W. Kuhn and F. Grün, Kolloid Z. 101, 248 (1942).
80. M. Doi and S. F. Edwards, "The Theory of Polymer Dynamics," Clarendon Press, Oxford, 1986.
81. N. Bloembergen, E. M. Purcell, and R. V. Pound, Phys. Rev. 73, 679 (1948).
82. P. W. Anderson and P. R. Weiss, Rev. Mod. Phys. 25, 269 (1953).
83. W. Kuhn, P. Barth, S. Hafner, G. Simon, and H. Schneider, Macromolecules 27, 5773 (1994).
84. W. Kühn, P. Barth, P. Denner, and R. Müller, Solid State Nucl. Magn. Reson. 6, 295 (1996).
85. R. Kimmich and G. Voigt, Z. Naturforsch. 23a, 1294 (1978).
86. R. Kimmich, G. Schnur, and M. Köpf, Progr. Nucl. Magn. Reson. Spectr. 20, 385 (1988).
87. P. Barth, S. Hafner, and P. Denner, Macromolecules 29, 1655 (1996) and references within.
88. P. Sotta, B. Deloche, J. Herz, A. Lapp, D. Durand, and J.-C. Rabadeux, Macromolecules 20, 2769 (1987).
89. J. P. Cohen-Addad, A. Viallat, and P. Guchot, Macromolecules 20, 2146 (1987).
90. M. Brereton, Macromolecules 22, 3667 (1989).
91. C. Fülber, "NMR-Relaxation und Bildgebung an Kautschuknetzwerken," Akademischer Verlag, München, 1996.
92. G. I. Sandakov, L. P. Smirnov, A. I. Sosikov, K. T. Summanen, and N. N. Volkova, J. Polym. Sci., Part B: Polym. Phys. Ed. 32, 1585 (1994).
93. C. Fülber, K. Unseld, V. Herrmann, K. H. Jacob, and B. Blümich, Colloid Polym. Sci. 274, 191 (1996).
94. A. O. K. Nieminen and J. L. Koenig, J. Adhes. Sci. Technol. 2, 407 (1988).
95. A. O. K. Nieminen, J. Liu, and J. L. Koenig, J. Adhes. Sci. Technol. 3, 455 (1989).
96. A. O. K. Nieminen and J. L. Koenig, Appl. Spectrosc. 43, 1358 (1989).
97. P. Jackson, N. J. Clayden, N. J. Walton, T. A. Carpenter, L. D. Hall, and P. Jezzard, Polym. Int. 24, 139 (1991).
98. T. G. Neiss and E. J. Vanderheiden, Macromol. Chem., Macromol. Symp. 86, 117 (1994).
99. J. M. Barton, G. J. Buist, I. Hamerton, J. H. Brendan, J. R. Jones, and S. Liu, Polym. Bull. 33, 215 (1994).
100. M. Knörgen, U. Heuert, H. Schneider, P. Barth, and W. Kuhn, Polym. Bull. 38, 101 (1997).
101. D. Hauck, G. Fink, C. Chwatinski. P. Blümler, B. Blümich, and K. Unseld, Kautsch. Gummi, Kunstst. 50(5), 392 (1997).
102. B. Blümich, P. Blümler, E. Günther, and G. Schauss, Bruker Report 2, 22 (1990).
103. P. Blümler and B. Blümich, Macromolecules 24, 2183 (1991).
104. S. Hafner and P. Barth, Magn. Reson. Imag. 13, 739 (1995).
105. P. Barth and S. Hafner, Magn. Reson. Imag. 14, (1996), in press.
106. W. Kuhn, E. Koeller, and I. Theis, in Ref. [9].
107. P. Blümler, B. Blümich, and H. Dumler, Kautsch. Gummi, Kunstst. 45, 699 (1992).
108. B. Blümich, P. Blümler, A. Guthausen, C. Fülber, G. Eidmann, and R. Savelsberg, Kautschuk-Herbst-Kolloquium, Hannover, Germany, Oct. 24-26, 1996.
109. A. Guthausen, "NMR-Bildgebung an Gummiformteilen," diploma thesis, RWTH-Aachen, 1996.
110. G. Simon, Polym. Bull. 25, 365 (1991).
111. B. Deloche and E. T. Samulski, Macromolecules 14, 575 (1981).
112. A. Dubault, B. Delroche, and J. Herz, Polymer 25, 1405 (1984).
113. M. G. Brereton, Macromolecules 24, 6160 (1991).
114. V. M. Litvinov and H. W. Spiess, Macromol. Chem. 192, 3005 (1991).
115. T. Nishi and T. Chikaraishi, J. Macromol. Sci.-Phys. B19, 445 (1981).
116. J. P. Cohen-Addad, P. Huchot, and A. Viallat, Polym. Bull. 19, 257 (1988).
117. K. Fukumori, N. Sato, A. Okada, and T. Kurauchi, Polym. Mater. Sci. Eng. 62, 649 (1990).
118. V. M. Litvinov and V. G. Vasilev, Polym. Sci. U.S.S.R. 32, 2231 (1990).
119. B. Blümich, P. Blümler, E. Günther, G. Schauss, and H. W. Spiess, Makromol. Chem. Macromol. Symp. 44, 37 (1991).
120. R. Stadler, M. M. Jacobi, and W. Gronski, Makromol. Chem. Rapid Commun. 4, 129 (1983).
121. M. Klinkenberg, P. Blümler, and B. Blümich, J. Magn. Reson. A 119, 197 (1996).
122. M. Klinkenberg, P. Blümler, and B. Blümich, Macromolecules 30(4), 1038 (1977).
123. W. Gronski, R. Stadler, and M. M. Jacobi, Macromolecules 17, 741 (1984).
124. M. M. Jacobi, R. Stadler, and W. Gronski, Macromolecules 19, 2884 (1986).
125. M. Hansen, B. Blümich, and H. W. Spiess, Macromolecules 25, 5542 (1992).
126. J. Miller, presented at the 3rd Int. Conf. Magn. Reson. Microsc., August 27-31, 1995, Würzburg, Germany.
127. E. Günther, B Blümich, and H. W. Spiess, Mol. Phys. 71, 477 (1990).
128. E. Günther, B. Blümich, and H. W. Spiess, Chem. Phys. Lett. 184, 251 (1991).
129. M. Cockman, L. Jelinski, J. Katz, D. Sorce, L. Boxt, and P. Cannon, J. Magn. Reson. 90, 9 (1990).
130. A. Abragam, "The Principles of Nuclear Magnetism," Oxford University Press, New York, 1961.
131. A. N. Garroway, J. Baum, M. G. Munowitz, and A. Pines, J. Magn. Reson. 60, 337 (1984).
132. A. Bax, R. Freeman, and S. B. Kempsell, J. Am. Chem. Soc. 102, 4849 (1980).
133. 2H-NMR an gedehnten Elastomeren," Shaker Vlg. Aachen, 1996.
134. R. Reiter, M. Stommel, and W. Michaeli, IKV-Aachen, FEM simulations and private communications.
135. P. T. Callaghan and E. T. Samulski, Macromolecules, 30, 113 (1997).
136. D. Hauck, P. Blümler, and B. Blümich, Macromol. Chem. Phys., 198, 2729 (1997).
137. J. A. Brydson, "Plastics Materials," fifth edition, Butterworths, London, 1989.
138. J. Zange, H. Adolf, R. Deichmann, U. Nöth, and A. Haase, J. Magn. Reson. B 106, 178 (1995).
139. S. J. Doran, T. A. Carpenter, and L. D. Hall, Rev. Sci. Instrum. 65, 2231 (1994).
140. L. R. G. Treolar, "The Physics of Rubber Elasticity," Clarendon Press, Oxford, 1975.
141. J. J. H. Ackerman, Concepts Magn. Reson. 2, 33 (1990).
142. J. B. Miller and A. N. Garroway, J. Magn. Reson. 77, 187 (1988).
143. J. B. Miller and A. N. Garroway, J. Magn. Reson. 85, 432 (1989).
144. F. Weigand, C. Fülber, B. Blümich, and H. W. Spiess, Magn. Reson. Imag. 12, 301 (1994).
145. G. A. Matzkanin in "Nondestructive Characterization of Materials," P. Höller, V. Hank, G. Dobmann, C. O. Ruud, and R. E. Green, Eds., Springer, Berlin, 1989.
146. G. Eidmann, R. Savelsberg, P. Blümler, and B. Blümich, J. Magn. Reson. A 122, 104 (1996).
147. R. L. Kleinberg, A. Sezginer, D. D. Griffin, and M. Fukuhara, J. Magn. Reson. 97, 466 (1992).
148. A. A. Samoilenko, D. Y. Artemov, and L. A. Sibeldina, JETP Lett. 47, 348 (1988).
149. J. B. Miller and A. N. Garroway, 35th Exp. NMR Conf., April 10-15, 1994, Pacific Grove, p. 186.
150. T. B. Benson and P. J. McDonald, J. Magn. Reson. A 112, 17 (1995).
151. Joel Miller, Naval Research Laboratory, Washington D.C., private communication.
152. R. Damadian, M. Goldsmith, and L. Minkoif, "NMR Basic Principles and Progress," Springer Verlag, Heidelberg, 1981, v. 19.
153. MARAN™ from Resonance Instruments Ltd.™, Oxbridge, UK.
154. Ralf Savelsberg, "NMR-Relaxationsuntersuchungen mit einem Oberflächenscanner an technischen Elastomeren," diploma thesis, RWTH-Aachen, 1996.
155. S. J. Gibbs and L. D. Hall, Meas. Sci. Technol. 7, 827 (1996).
156. G. Neue, NRW Symposium 1996, Aachen, Germany.
157. R. Dagani, Chem. Eng. News 74(36), 9 (1996).
158. A web page with currently updated NMR imaging results can be found under http:\\www.mc.rwthaachen.de\~bluemler\gallery.htm.