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note
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All data were collected at 85 K in the θ -2θ scan mode. Data were corrected for Lorentz and polarization effects and for secondary extinction but not for absorption. Programs used in this work include locally modified versions of the following: CARESS (Broach, Coppens, Becker, and Blessing), peak profile analysis and Lorentz and polarization correction; SHELX86 (Sheldrick), a crystal structure solution package; ORTEP (Johnson). All calculations were performed on a VAX 3100 computer in the J. D. McCullough X-ray Crystallography Laboratory.
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