Determination of fumonisins B1 and B2 and their major hydrolysis products in corn, feed, and meat, using HPLC

Journal of Agricultural and Food Chemistry

Volumn 44, Issue 4, 1996, Pages 1047-1052

  Thakur, Rohan A ^a   Smith, J Scott ^a  

^a KANSAS STATE UNIVERSITY   (United States)

Author keywords

Fumonisins; HPLC; Hydrolysis; Mass spectrometry; Metabolites

Indexed keywords

ZEA MAYS;

EID: 0001444866     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf950363w     Document Type: Article

References (24)

1. 3 by using cholera toxin as the carrier-adjuvant. Appl. Environ. Microbiol. 1992, 58, 169-173.
2. Bader, M. A systematic approach to standards addition methods in instrumental analysis. J. Chem. Educ. 1980, 57, 703-706.
3. Bezuidenhout, C. S.; Gelderblom, W. C. A.; Gorst-Allman, P. C.; Horak, M. R.; Marasas, W. F. O.; Spiteller, G.; Vleggaar, R. Structure elucidation of the fumonisins, mycotoxins from Fusarium moniliforme. J. Chem. Soc., Chem. Commun. 1988, 743-745.
4. Cronin, J. R.; Pizzarello, S.; Gandy, W. E. Amino acid analysis with o-phthalaldehyde detection: effects of reaction temperature and thiol on fluorescence yields. Anal. Biochem. 1978, 93, 174-179.
5. Doerge, D. R.; Howard, P. C.; Bajic, S.; Preece, S. Determination of fumonisins using on-line liquid chromatography coupled to electrospray mass spectrometry. Rapid Commun. Mass Spectrom. 1994, 8, 603-606.
6. Dolan, J. W. Obtaining separations, part I: a look at retention. LC-GC 1994, 12, 368-370.
7. Gelderblom, W. C. A.; Jaskiewicz, K.; Marasas, W. F. O.; Thiel, P. G.; Horak, R. M.; Vleggaar, R.; Kriek, N. P. J. Fumonisins-novel mycotoxins with cancer promoting activity produced by Fusarium moniliforme. Appl. Environ. Microbiol. 1988, 54, 1806-1811.
8. 1 in rats. Carcinogenesis 1991, 12, 1247-1251.
9. 1 a toxic metabolite of Fusarium moniliforme. J. Vet. Diagn. Invest. 1990, 2, 217-221.
10. Hendrich, S.; Miller, K. A.; Wilson, T. M.; Murphy, P. A. Toxicity of Fusarium proliferatum-fermented nixtamalized corn-based diets fed to rats: effect of nutritional status. J. Agric. Food Chem. 1993, 41, 1649-1654.
11. 1 in corn-containing foods. J. Agric. Food Chem. 1993, 41, 1655-1658.
12. Plattner, R. D.; Norred, W. P.; Bacon, C. W.; Voss, K A.; Paterson, R.; Schackelford, D. D.; Weisleder, D. A method associated with detection of fumonisins in corn samples associated with field cases of equine leukoencephalomalacia. Mycologia 1990, 82, 698-702.
13. Rice, L. G.; Ross, F. P. Methods for detection and quantitation of fumonisins in corn, cereal products, and animal excreta. J. Food Prot. 1994, 57, 536-540.
14. Rice, L. G.; Ross, F. P.; Dejong, J.; Plattner, R. D.; Coats, J. Evaluation of liquid chromatographic method for the determination of fumonisins in corn, poultry feed, and Fusarium culture material. J. AOAC Int. 1995, 78, 1002-1009.
15. 1 in feeds associated with animal health problems. Mycopathologia 1991, 114, 129-135.
16. Ross, F. P.; Rice, L. G.; Ledet, A. E.; Owens, D. L.; Nelson, H. A.; Osweiler, G. D.; Wilson, T. M. Experimental equine leukoencephalomalacia, toxic hepatosis, and encephalopathy caused by corn naturally contaminated with fumonisins. J. Vet. Diagn. Invest. 1993, 5, 69-74.
17. Scott, P. M.; Lawrence, G. A. Liquid chromatographic determination of fumonisins with 4-fluoro-7-nitrobenzofuran. J. AOAC Int. 1992, 75, 829-834.
18. 2 by high-performance liquid chromatography with fluorescence detection. J. Lig. Chromatogr. 1990, 13, 2077-2087.
19. 1 in plasma and urine by high-performance liquid chromatography. J. Chromatogr. 1992, 574, 299-304.
20. 1 and the identification of its partially hydrolyzed metabolites in the feces of non-human primates. Food Chem. Toxicol. 1994, 32, 23-31.
21. Smith, J. S.; Thakur, R. A. Fate and analysis of fumonisins in beef. In Fumonisins in Food; L. Jackson, DeVries, J. W., and Bullerman, L. B., Eds.; Plenum Press: New York, 1996; Chapter 4.
22. 1 by negative-ion thermospray mass spectrometry. Rapid Commun. Mass Spectrom. 1994, 8, 82-88.
23. 2 in corn: IUPAC collaborative study. J. AOAC Int. 1993, 76, 361-366.
24. Wilson, T. M.; Ross, F. P.; Owens, D. L.; Rice, L. G.; Green, S. A.; Jenkins, S. J.; Nelson, H. A. Experimental reproduction of ELEM. Mycopathalogia 1992, 11, 115-120.