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Volumn 96, Issue 8, 1996, Pages 3241-3267

Synthesis and reactivity of sp3-geminated organodimetallics

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Indexed keywords


EID: 0001408339     PISSN: 00092665     EISSN: None     Source Type: Journal    
DOI: 10.1021/cr9600161     Document Type: Article
Times cited : (269)

References (252)
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    • note
    • Whatever the structure of the organometallic species involved, it has been established that 2 mol equiv of magnesium iodide were required.
  • 71
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    • note
    • The solution of the di-Grignard compound is remarkably stable, the titre being practically unchanged after storing at 0 °C for several weeks or after boiling at reflux for 15 min.
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    • (b) Carr, D. B.; Schwartz, J. J. Am. Chem. Soc. 1979, 101, 3521 and references cited therein.
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    • Carr, D.B.1    Schwartz, J.2
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    • (d) For a more recent review, see: Charette, A. B.; Marcoux, J. F, Synlett 1995, 1197 and references cited therein.
    • (1995) Synlett , pp. 1197
    • Charette, A.B.1    Marcoux, J.F.2
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    • US Patent 3 865 848, 1975
    • Nysted, L. N. US Patent 3 865 848, 1975; Chem. Abstr. 1975, 83, 10406q. This reagent is commercially available from Aldrich Co.
    • (1975) Chem. Abstr. , vol.83
    • Nysted, L.N.1
  • 195
    • 0000784042 scopus 로고
    • Trost, B., Fleming, I., Eds.; Pergamon Press: New York
    • (d) Oppolzer, W. Comprehensive Organic Synthesis; Trost, B., Fleming, I., Eds.; Pergamon Press: New York, 1991; Vol. 5, p 28.
    • (1991) Comprehensive Organic Synthesis , vol.5 , pp. 28
    • Oppolzer, W.1
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    • Trost, B.; Fleming, I., Eds.; Pergamon Press: New York
    • (e) Roush, W. Comprehensive Organic Synthesis; Trost, B.; Fleming, I., Eds.; Pergamon Press: New York, 1991; Vol. 2, p 1.
    • (1991) Comprehensive Organic Synthesis , vol.2 , pp. 1
    • Roush, W.1
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    • and references cited therein
    • (b) Ma, S.; Lu, X. Org. Synth. 1994, 72, 112 and references cited therein.
    • (1994) Org. Synth. , vol.72 , pp. 112
    • Ma, S.1    Lu, X.2
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    • 0003065849 scopus 로고
    • Trost, B., Fleming, I., Eds.; Pergamon Press: New York
    • (b) Yamamoto, H. Comprehensive organic synthesis; Trost, B., Fleming, I., Eds.; Pergamon Press: New York, 1991; Vol. 2, p 81.
    • (1991) Comprehensive Organic Synthesis , vol.2 , pp. 81
    • Yamamoto, H.1
  • 246
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    • note
    • It was considered that the carbon-metal bond reacts with retention of configuration with each electrophile as is usual in the case of nonallylic or nonbenzylic organometallics. See ref 151.


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