Synthesis of Cp′2Ta(SH)H2 from Cp′2Ta(=S)H (Cp′ = η5-t-BuC5H4) and its application in the preparation of new hydrosulfido-bridged heterobimetallic complexes

New Journal of Chemistry

Volumn 21, Issue 8, 1997, Pages 903-908

  Challet, Sylvine ^a   Blacque, Olivier ^a   Gehart, Günther ^a   Kubicki, Marek M ^a   Leblanc, Jean Claude ^a   Moïse, Claude ^a   Brunner, Henri ^b   Wachter, Joachim ^b  

^a UNIVERSITÉ DE BOURGOGNE   (France)

^b UNIVERSITY OF REGENSBURG   (Germany)

Author keywords

EHMO; Heterobimetallic complexes; Hydrosulfide bridge; Tantalum; X ray analysis

Indexed keywords

EID: 0001403333     PISSN: 11440546     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (57)

1. Wachter J., Angew. Chem. Int. Ed. Engl., 1989, 28, 1613;
2. Kanatzidis M. G., Huang S-P., Coord. Chem. Rev., 1994, 130, 509;
3. Fenske D., Ohmer J., Hachgenei J., Merzweiler K., Angew. Chem. Int. Ed. Engl., 1988, 27, 1277;
4. Shibahara T., Coord. Chem. Rev., 1993, 123, 73.
5. (a) Herrmann W. A., Angew. Chem. Int. Ed. Engl., 1986, 25, 56;
6. (b) Brunner H., Challet S., Kubicki M. M., Leblanc J-C., Moïse C., Volpato F., Wachter J., Organometallics, 1995, 14, 3623;
7. (c) Kubicki M. M., Oudet P., Martin C., Barré C., J. Chem. Soc., Dalton Trans., 1995, 3699;
8. (d) Sellmann D., Weiß R., Knoch F., Moll M., J. Organomet. Chem., 1990, 391, 327;
9. (e) Goh L. Y., Tay M. S., Lim Y. Y., Chen W., Zhou Z-Y., Mak T. C. W., J. Organomet. Chem., 1992, 441, 51;
10. (f) Höfler M., Hausmann H., Heidelberg H. A., J. Organomet. Chem., 1981, 213, C1;
11. (g) Brunner H., Gehart G., Leblanc J-C., Moïse C., Nuber B., Stubenhofer B., Volpato F., Wachter J., J. Organomet. Chem., 1996, 517, 47.
12. See for example: Erker G., Albrecht M., Psiorz C., Z. Naturforsch (B), 1991, 46, 1571;
13. Evans W. J., Rabe G. W., Ziller J. W., Doedens R. J., Inorg. Chem., 1994, 33, 2719;
14. El-Hinnawi M. A., Aruffo A. A., Santarsiero B. D., McAlister D. R., Schomaker V., Inorg. Chem., 1983, 22, 1585;
15. Brennan J. G., Andersen R. A., Zalkin A., Inorg. Chem., 1986, 25, 1761;
16. Berg D. J., Burns C. J., Andersen R. A., Zalkin A., Organometallics, 1989, 8, 1865;
17. Jemmis E. D., Pavan Kumar P. N. V., Narahari Sastry G., J. Organomet. Chem., 1994, 478, 29;
18. Beuter G., Drobnik S., Lorenz I.-P., Lubik A., Chem. Ber., 1992, 125, 2363;
19. Herberhold M., Jellen W., Murray H. H., J. Organomet. Chem., 1984, 270, 65;
20. Abel E. W., Evans D. G., Koe J. R., Hursthouse M. B., Mazid M., Mahon M. F., Molloy K. C., J. Chem. Soc., Dalton Trans., 1990, 1697;
21. Hofreiter S., Paul M., Schmidbaur H., Chem. Ber., 1995, 128, 901.
22. (a) Kowacs J. A., Bergman R. G., J. Am. Chem. Soc., 1989, 111, 1131;
23. (b) Massa M. A., Rauchfuss T. B., Wilson S. R., Inorg. Chem., 1991, 30, 4667;
24. (c) Guerchais J. E., LeQuèré J. L., Petillon F. Y., Manojlovic-Muir L., Muir K. W., Sharp D. W. A., J. Chem. Soc., Dalton Trans., 1982, 283.
25. (a) Nelson J. E., Parkin G., Bercaw J. E., Organometallics, 1992, 11, 2181;
26. (b) Housmekeredis C. E., Ramage D. L., Kretz C. M., Shontz J. T., Pilato R. S., Geoffroy G. L., Rheingold A. L., Haggerty B. S., Inorg. Chem., 1992, 31, 4453;
27. (c) Pilato R. E., Eriksen K. A., Stiefel E. I., Rheingold A. L., Inorg. Chem., 1993, 32, 3799;
28. (d) Howard W. A., Parkin G., J. Am. Chem. Soc., 1994, 116, 606;
29. (e) Shin J. H., Parkin G., Organometallics, 1995, 14, 1104;
30. (f) Coucouvanis D., Al-Ahmad S., Kim C. G., Koo S-M., Inorg. Chem., 1992, 31, 2996;
31. (g) Tatsumi K., Inoue Y., Kawaguchi H., Kohsaka M., Nakamura A., Cramer R. E., VanDoorne W., Taogoshi G. J., Richmann P. N., Organometallics, 1993, 12, 352;
32. (h) Kuchta M. C., Parkin G., J. Am. Chem. Soc., 1994, 116, 8372;
33. (i) Carney M. J., Walsh P. J., Hollander F. G., Bergman R. G., Organometallics, 1992, 11, 761.
34. Brunner H., Kubicki M. M., Leblanc J-C., Moïse C., Volpato F., Wachter J., J. Chem. Soc., Chem. Commun., 1993, 851.
35. Mugnier Y., private communication.
36. (a) Hoffmann R. J., J. Chem. Phys., 1963, 39, 1397;
37. (b) Hoffmann R. J., Lipscomb W. N. J., Chem. Phys., 1962, 36, 2179;
38. (c) Ammeter J. H., Burgi H. B., Thibeault J. C., Hoffmann R. J., J. Am. Chem. Soc., 1978, 100, 3686;
39. (d) Mealli C., Proserpio D. M., J. Chem. Ed., 1990, 67, 399.
40. (a) Ozawa Y., de Miguel A. V., Isobe K., J. Organomet. Chem., 1992, 433, 183;
41. (b) Amarasekera J., Rauchfuss T. B., Inorg. Chem., 1989, 28, 3875;
42. (c) Mueting A. M., Boyle P., Pignolet L. H., Inorg. Chem., 1984, 23, 44;
43. (d) Danzer W., Fehlhammer W. P., Liu A. T., Thiel G., Beck W., Chem. Ber., 1982, 115, 1682;
44. (e) Bianchini C., Mealli C., Meli A., Sabat M., Inorg. Chem., 1986, 25, 4617;
45. (f) Hashizume K., Mizobe Y., Hidai M., Organometallics, 1996, 15, 3303;
46. (g) Skripkin Y. V., Eremenko I. L., Pasynskii A. A., Struchkov Y. T., Shklover V. E., J. Organometal. Chem., 1984, 267, 285;
47. (h) Herrmann W. A., Biersack H., Ziegler M. L., Balbach B., J. Organomet. Chem., 1981, 206, 35;
48. (i) Casewit C. J., Rakowski DuBois M., J. Am. Chem. Soc., 1986, 108, 5482.
49. Ruffing C. J., Rauchfuss T. H., Organometallics, 1985, 4, 524.
50. (a) Oudet P., Perrey D., Bonnet G., Moïse C., Kubicki M. M., Inorg. Chim. Acta, 1995, 237, 79;
51. (b) Bonnet G., Kubicki M. M., Lavastre O., Leblanc J. C., Moïse C., Acta Crystallogr., Sect. A, Suppl., 1990, C227;
52. (c) Barré C., Kubicki M. M., Leblanc J.-C., Moïse C., Inorg. Chem., 1990, 29, 5244;
53. (d) Shyu S-G., Hsu J.-Y., Lin P.-J., Wu W.-J., Peng S.-M., Lee G.-H., Wen Y.-S., Organometallics, 1994, 13, 1699.
54. Bach H.-J., Brunner H., Wachter J., Kubicki M. M., Leblanc J.-C., Moïse C., Volpato F., Nuber B., Ziegler M. L., Organometallics, 1995, 11, 1403.
55. Fair C. K., MOLEN, Structure Determination System, Enraf-Nonius, Delft, 1990.
56. Cromer D. T., Waber J. T., International Tables for X-ray Crystallography, Vol. IV, Kynoch, Birmingham, 1975.
57. Walker N., Stuart D., Acta Crystallogr., Sect. A, 1983, 39, 158.