Preparation and X-ray crystal structure of a unique 2:1-complex of mercury(II) chloride and 5-oxa-2,8-dithiabicyclo[7.4.1]tetradeca-9,11,13-trien-14-one, a troponoid dithio-crown ether

Heterocycles

Volumn 47, Issue 1, 1998, Pages 149-152

  Mori, Akira ^a   Kubo, Kanji ^b   Kato, Nobuo ^a   Takeshita, Hitoshi ^c   Shiono, Masaaki ^a   Achiwa, Norio ^a  

^a KYUSHU UNIVERSITY   (Japan)

^b KANAGAWA UNIVERSITY   (Japan)

^c TOHWA UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001359764     PISSN: 03855414     EISSN: None     Source Type: Journal    
DOI: 10.3987/COM-97-S(N)56     Document Type: Article

References (23)

1. (a) N. K. Dalley and S. B. Larson, Acta Cryst., 1981, B37, 2225;
2. (b) N. Galesic, M. Herceg, and D. Sevdic, Acta Cryst., 1986, C42, 565;
3. (c) A. J. Blake and M. Schröder, Adv. Inorg. Chem., 1990, 35, 1 and references cited therein;
4. (d) G. Wu, W. Jiang, J. D. Lamb, J. S. Bradshaw, and R. M. Izatt, J. Am. Chem. Soc., 1991, 113, 6538;
5. (e) M. Herceg and D. Matkovic-Calogovic, Acta Cryst., 1992, C48, 1779;
6. (f) K. A. Byriel, L. R. Gahan, C. H. L. Kennard, and C. J. Sunderland, J. Chem. Soc., Chem. Commun., 1993, 625;
7. (g) J. W. Sibert, S. J. Lange, C. Stern, B. M. Hoffman, and A. G. M. Barrett, J. Chem. Soc., Chem. Commun., 1994, 1751.
8. (a) B. de Groot and S. J. Loeb, J. Chem. Soc., Chem. Commun., 1990, 1755;
9. (b) A. J. Blake, G. Reid, and M. Schröder, J. Chem. Soc., Dalton Trans., 1990, 3849;
10. (c) A. J. Blake, G. Reid, and M. Schröder, J. Chem. Soc., Chem. Commun., 1992, 1074.
11. (a) H. Takeshita, A. Mori, and S. Hirayama, J. Chem. Soc., Chem. Commun., 1989, 564;
12. (b) K. Kubo, A. Mori, and H. Takeshita, Chem. Express, 1992, 7, 945;
13. H. Takeshita, B. Z. Yin, K.
14. (a) K. Kubo, A. Mori, and H. Takeshita, Heterocycles, 1993, 36, 1941;
15. (b) A. Mori, K. Kubo, and H. Takeshita, Bull. Chem. Soc. Jpn., 1994, 67, 1094.
16. 2)]=0.0488
17. V. Subramanian and K. Seff, Acta Cryst., 1980, B36, 2132.
18. P. Biscarini, L. Fusina, G. D. Nivellini, A. Mangia, and G. Pelizzi, J. Chem. Soc., Dalton Trans., 1974, 1846.
19. D. Grdenic, Quart. Rev. Chem. Soc., 1965, 19, 303.
20. Y. Kawasaki and Y. Matsuura, Chem. Lett., 1984, 155.
21. 2)]=0.0781
22. We discussed the bond lengths and the bond angles of one of the two independent molecules.
23. G. M. Sheldrick, 'SHELXL93. Program for the Refinement of Crystal Structures,' University of Göttingen, Germany, 1993.