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The 30% were counted with respect to the original covered area. It is the decrease in size of each dot, whatever area of the hydrophilic region. The 60% were determined with respect to the area of the hydrophilic SAM; this means that the colloidal suspensions did not cover the entire hydrophilic area after dewetting.
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40
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50
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85033829520
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note
-
In the "tapping mode", the cantilever is oscillated with a high amplitude (≈20 nm) near its resonance frequency and moved toward the surface of the sample until it begins to tap the surface; the topography is obtained directly by measuring the voltage required at the Z piezo to keep the amplitude of the oscillation of the cantilever constant.
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51
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85033827190
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note
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The Nanoscope III uses an ac method for magnetic force detection which tracks shifts m the resonance properties (amplitude and phase) of an oscillating cantilever. The resonance frequency is decreased when the magnetic interaction is attractive and increased when it is repulsive. We used the phase detection mode at a constant driving frequency. Resonance shifts give rise to phase shifts which give an image of the magnetic force gradients.
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