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Volumn 37, Issue 24, 1998, Pages 6136-6146

1,3,5-Triamino-1,3,5-trideoxy-cis-inositol and all-cis-2,4,6-Trimethoxycyclohexane-1,3,5-triamine as Building Blocks for New Multidentate and Macrocyclic Ligands 1

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EID: 0001303896     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic980483w     Document Type: Article
Times cited : (19)

References (60)
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    • note
    • 3+ (6).
  • 3
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    • Wilkinson, G., Ed.; Pergamon Press: Oxford, U.K.
    • (b) House, D. A. Comprehensive Coordination Chemistry; Wilkinson, G., Ed.; Pergamon Press: Oxford, U.K., 1987; Vol. 2, pp 23-72.
    • (1987) Comprehensive Coordination Chemistry , vol.2 , pp. 23-72
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  • 12
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    • (1992) Angew. Chem. , vol.104 , pp. 542-563
    • Seel, C.1    Vögtle, F.2
  • 13
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    • Seel, C.; Vögtle, F. Angew. Chem. 1992, 104, 542-563; Angew. Chem., Int. Ed. Engl. 1992, 31, 528.
    • (1992) Angew. Chem., Int. Ed. Engl. , vol.31 , pp. 528
  • 37
    • 85088543223 scopus 로고    scopus 로고
    • note
    • 2O, this signal disappeared upon heating the sample. In addition, the signal at 2.85 ppm now appeared as a sharp triplet (J = 3.8 Hz).
  • 38
    • 85088543596 scopus 로고    scopus 로고
    • note
    • 3. Shorter or longer reaction times resulted in a significantly diminished yield.
  • 41
    • 0003528602 scopus 로고
    • Molecular Structure Corporation: The Woodlands, TX
    • teXsan Crystal Structure Analysis Package; Molecular Structure Corporation: The Woodlands, TX, 1985 and 1992.
    • (1985) TeXsan Crystal Structure Analysis Package
  • 48
    • 85088543579 scopus 로고    scopus 로고
    • note
    • o) = esd based on counting statistics.
  • 51
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    • note
    • 13C).
  • 52
    • 85088542231 scopus 로고    scopus 로고
    • note
    • w = 6.43% for 813 observed reflections [I > 2ω(I)] and 227 refined parameters. The mean Co-N distance is 1.96(1) Å.
  • 56
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    • Ph.D. Thesis, Australian National University
    • (b) Walker, G. W. Ph.D. Thesis, Australian National University, 1997.
    • (1997)
    • Walker, G.W.1
  • 57
    • 0001016088 scopus 로고
    • 3+ (en = ethane1,2-diamine), formaldehyde, and nitromethane rapidly produced the bicapped complex whereas for the corresponding analogue with the more rigid trans-cyclohexane-1,2-diamine ligand, the reaction proceeded more slowly and in equivalent conditions only the monocapped species was formed: Geue, R. J.; McCarthy, M. G.; Sargeson, A. M. J. Am. Chem. Soc. 1984, 106, 8282.
    • (1984) J. Am. Chem. Soc. , vol.106 , pp. 8282
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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.