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Tetrahedron Letters
Volumn 29, Issue 46, 1988, Pages 5871-5874
Simultaneous multiple synthesis of protected peptide fragments on 'allyl'-functionalized cellulose disc supports
Author keywords

[No Author keywords available]
Indexed keywords

EID: 0001271842     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(00)82212-1     Document Type: Article
Times cited : (59)
References (15)
  • 1
    • 84918453799 scopus 로고    scopus 로고
    • R. Frank and R. Döring, Tetrahedron, in press.
  • 10
    • 0009277236 scopus 로고
    • Festphasen-Synthese von Peptiden und Glycopeptiden an polymeren Trägern mit allylischen Ankergruppen
    • (1988) Angewandte Chemie , vol.100 , pp. 732
    • Kunz1    Dombo2
  • 11
    • 84918453798 scopus 로고    scopus 로고
    • Special abbreviations used: Ac, acetyl; DCA, dichloroacetic acid; FAB, fast atom bombardment; Fmoc, 9-fluorenylmethoxycarbonyl; HOBt, N-hydroxybenzotriazole; HPLC, high pressure liquid chromatography; MeOH, methanol; MeOTr-, 4-methoxy trityl; MSNT, mesitylenesulfonyl- 3-nitro-1,2,4-triazole; TEA, triethylamine; TFA, trifluoroacetic acid; THF, tetrahydrofuran; TLC, thin layer chromatography.
  • 12
    • 84918453797 scopus 로고    scopus 로고
    • 3): δ = 7.446 [m; H- 2′/H-6′], 7.328 [“d”; H-2″/H-6″; J(2″-3″)+J(2“-5”) 9.0], [[Truncated]]
  • 13
    • 84918453796 scopus 로고    scopus 로고
    • 2/MeOH/TEA (94.5 : 5; 0.5 by volume) as solvent. 4″-Monomethoxytrityl-6-, 1′,4′ [[Truncated]]
  • 14
    • 84918453795 scopus 로고    scopus 로고
    • About 10 μg of material from an HPLC peak fraction was evaporated to dryness and dissolved in 10 μl dioxane. A 2 to 3 μl aliquot was injected into a droplet of 3-nitrobenzyl alcohol as matrix on the sample tip. Mass spectra were recorded on a Kratos MS 50RF with a high field magnet (mass range ca. 10.000 at 8 kV) and a Kratos FAB source using a beam of neutral xenon atoms at 8–9 kV.

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.