Synthesis, structure, and coordination chemistry of a tridentate, six-electron-donor amidinate ligand

Organometallics

Volumn 18, Issue 25, 1999, Pages 5360-5366

  Kincaid, Kristi ^a   Gerlach, Christopher P ^a   Giesbrecht, Garth R ^a   Hagadorn, John R ^a   Whitener, Glenn D ^a   Shafir, Alex ^a   Arnold, John ^a  

^a NONE

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001257723     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om990365w     Document Type: Article

References (32)

1. Edelmann, F. T. Coord. Chem. Rev. 1994, 137, 403.
2. Barker, J.; Kilner, M. Coord. Chem. Rev. 1994, 133, 219.
3. Hagadorn, J. R.; Arnold, J. Angew. Chem., Int. Ed. Engl. 1998, 37, 1729.
4. Whitener, G D.; Hagadorn, J. R.; Arnold, J. J. Chem. Soc., Dalton. Trans. 1999, 1249.
5. During the preparation of this article, the synthesis of an amidinate ligand with a pendant dimethylamino group was described: (a) Brandsma, M. J. R.; Brussee, E. A. C.; Meetsma, A.; Hessen, B.; Teuben, J. H. Eur. J. Inorg. Chem. 1998, 1867. An amidinate ligand with a noncoordinating dimethylamino group has also been reported: (b) Hao, S.; Gambarotta, S.; Bensimon, C.; Edema, J. J. H. Inorg. Chim. Acta 1993, 213, 65.
6. During the preparation of this article, the synthesis of an amidinate ligand with a pendant dimethylamino group was described: (a) Brandsma, M. J. R.; Brussee, E. A. C.; Meetsma, A.; Hessen, B.; Teuben, J. H. Eur. J. Inorg. Chem. 1998, 1867. An amidinate ligand with a noncoordinating dimethylamino group has also been reported: (b) Hao, S.; Gambarotta, S.; Bensimon, C.; Edema, J. J. H. Inorg. Chim. Acta 1993, 213, 65.
7. Boere, R. T.; Klassen, V.; Wolmershauser, G. J. Chem. Soc., Dalton Trans. 1998, 4147.
8. Boyd, G. V. In The Chemistry of Arnidines and Imidates; Patai, S., Rappoport, Z., Eds.; John Wiley & Sons: Chichester, 1991; Vol. 2, pp 339-366.
9. Silverstein, R. M.; Bassler, G. C.; Morrill, T. C. Spectrometric Identification of Organic Compounds; John Wiley & Sons: New York, 1991.
10. Hafelinger, G.; Kuske, K. H. In The Chemistry of Amidines and Imidates; Patai, S., Rappoprt, Z., Eds.; John Wiley & Sons: Chichester, 1991; Vol. 2, pp 1-100.
11. Srinivas, B.; Chang, C. C.; Chen, C. H.; Chiang, M. Y.; Chen, I. T.; Wang, Y.; Lee, G. H. J. Chem. Soc., Dalton Trans. 1997, 957.
12. Westerhausen, M.; Hausen, H. D. Z. Anorg. Allg. Chem. 1992, 615, 27.
13. Coles, M. P.; Swenson, D. C.; Jordan, R. P.; Young, V. G. Organometallics 1997, 16, 5183.
14. Coles, M. P.; Swenson, D. C.; Jordan, R. F.; Young, V. G. Organometallics 1998, 17, 4042.
15. Lechler, E.; Hausen, H. D.; Weidlin, J. J. Organomet. Chem. 1989, 359, 1.
16. Vranka, R. G.; Amma, E. L. J. Am. Chem. Soc. 1967, 89, 3121.
17. Scholz, J.; Rehbaum, F.; Thiele, K. H., Goddard, R.; Betz, P.; Kruger, C. J. Organomet. Chem. 1993, 443, 93.
18. Walther, D.; Fischer, R.; Gorls, H.; Koch, J.; Schweder, B. J. Organomet. Chem. 1996, 508, 13.
19. Hagadorn, J. R.; Arnold, J. J. Chem. Soc., Dalton Trans. 1997, 3087.
20. Gagne, M. S.; Stern, C. L.; Marks, T. J. J. Am. Chem. Soc. 1992, 114, 275.
21. Bradley, D C.; Ghotra, J. S.; Hart, F. A.; Hursthouse, M. B.; Raithby, P. R. J. Chem. Soc., Dalton Trans. 1977, 1166.
22. Shriver, E. F.; Bredzon, M. A. The Manipulation of Air-Sensitive Compounds; John Wiley & Sons: New York, 1986.
23. Pangborn, A. B.; Giardello, M. A.; Grubbs, R. H.; Rosen, R. K.; Timmers, F. J. Organometallics 1996, 15, 1518.
24. Magnus, G.; Levine, R. J. Am. Chem. Soc. 1956, 78, 4127
25. Zucchini, U.; Giannini, U.; Albizatti, E.; D'Angelo, R. Chem. Commun. 1969, 1174.
26. Zucchini, U.; Giannini, U.; Albizzati, E. J. Organomet. Chem. 1971, 26, 357.
27. Evans, W. J.; Golden, R. E.; Ziller, J. W. Inorg. Chem. 1991, 30, 4963.
28. SMART Area-Detector Software Package; Madison, WI, 1993.
29. SAINT: SAX Area-Detector Integration Program; Madison, WI, 1995.
30. XPREP: Part of the SHELXTL Crystal Structure Determination Package; Madison, WI, 1995.
31. TeXsan: Crystal Structure Analysis Package; Molecular Structure Corporation: The Woodlands, TX, 1992.
32. SIR92: Altomare, A.; Burla, M. C.; Camilli, M.; Cascarano, M.; Giacovazzo, C.; Guagliardi, A., Polidori, G. J. Appl. Crystallogr. 1993, 26, 343.