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Volumn 27, Issue 34, 1986, Pages 4025-4028

Me3SiCl/HMPA accelerated conjugate addition of catalytic copper reagent. Stereoselective synthesis of enol silyl ether of aldehyde

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Indexed keywords


EID: 0001249846     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(00)84901-1     Document Type: Article
Times cited : (238)

References (26)
  • 6
    • 84918130355 scopus 로고    scopus 로고
    • Abstracts, 32nd Symposium on Organometallic Chemistry, Japan; November 6, Suita: B214.
  • 11
    • 84918130354 scopus 로고    scopus 로고
    • 4. The 1,4-adduct (3.86 g, 83%; 94% E by GLC analysis) was obtained as an enol silyl ether by distillation (74 °C, 1 mm Hg).
  • 12
    • 85077870910 scopus 로고
    • Organocopper Conjugate Addition-Enolate Trapping Reactions
    • (1985) Synthesis , pp. 364
    • Taylor1
  • 13
    • 84918130353 scopus 로고    scopus 로고
    • 3SiF.
  • 15
    • 84918130352 scopus 로고    scopus 로고
    • TMSCl/HMPA did not show favorable effects in the reaction with epoxides and 1,1-dialkoxycarbonylcyclopropane.
  • 16
    • 84918130351 scopus 로고    scopus 로고
    • 3SiCI and triethylamine was used in situ to increase the product yield (ref 4).
  • 25
    • 84918130350 scopus 로고    scopus 로고
    • 1H NMR coupling constant and/or NOE studies.
  • 26
    • 84918130349 scopus 로고    scopus 로고
    • 3SiCl from Toray Silicone are deeply acknowledged.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.