A One-Step Method for the Synthesis of a Vinyl-Containing Silsesquioxane and Other Organolithic Macromolecular Precursors

Inorganic Chemistry

Volumn 35, Issue 1, 1996, Pages 261-262

  Yuchs, Steven E ^a   Carrado, Kathleen A ^a  

^a ARGONNE NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001188169     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic950356p     Document Type: Article

References (18)

1. (a) Day, V. W.; Klemperer, W. G.; Mainz, V. V.; Millar, D. M. J. Am. Chem. Soc. 1985, 107, 8262-4.
2. (b) Feher, F. J.; Weller, K. J. Inorg. Chem. 1991, 30, 882-3.
3. (c) Feher, F. J.; Weller, K. J. Chem. Mater. 1994, 6, 7-9.
4. (d) Agaskar, P. A. Inorg. Chem. 1990, 29, 1603.
5. (e) Agaskar, P. A. J. Chem. Soc., Chem. Commun. 1991, 1024-6.
6. (f) Feher, F. J.; Weller, K. J. Organametallics 1990, 9, 2638-40.
7. (g) Feher, F. J.; Budzichowski, T. A.; Weller, K. J. J. Am. Chem. Soc. 1989, 111, 7288-9.
8. Frye, C. L.; Collins, W. T. J. Am. Chem. Soc. 1970, 92, 5586-8.
9. Feher, F. J.; Newman, D. A.; Walzer, J. F. J. Am. Chem. Soc. 1989, 111, 1741-8.
10. Moran, M.; Casado, M.; Cuadrado, I.; Losada, J, Qrganometallics 1993, 12, 4327-33.
11. 1.4
12. -1): 2963, 1597, 1254, 1008, 559.
13. 3), -109.43 (Si core). IR (in KBr; cm-1): 2902. 1785, 1450, 1225, 1072, 842, 557.
14. -1): 3463, 2959, 1748, 1640, 1438, 1260, 1097, 852, 806, 453.
15. (a) Hoebbel, D.; Pitsch, L; Heidemann, D.; Jancke, H.; Miller, W. Z. Anorg. Allg. Chem. 1990, 583, 133-44.
16. (b) Hoebbel, D.; Endres, K.; Reinert, T.; Schmidt, H. In Better Ceramics Through Chemistry VI; Cheetam, A. K., Brinker, C. J., Mecarmey, M. L., Sanchez, C., Eds.; Materials Research Society: San Francisco, CA, 1994; p 863.
17. Agaskar, P. A. J. Chem. Soc., Chem. Commun. 1992, 1024-6.
18. Sol-Gel Technology for Thin Films, Fibers, Preforms, Electronics, and Speciality Shapes; Klein, L. C., Ed.; Noyes: Park Ridge, NJ, 1988.