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23
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27844530285
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note
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2O, 25°C) δ (ppm): 130.62 (C-H arom); 134.92 (C arom); 167.81 (C amidine).
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-
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24
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84984085993
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Bosshard H. H., Mory R., Schmid M., Zollinger Hch., Helv. Chim. Acta, 1959, 42, 1653-1658.
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26
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0000483322
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Henn, B.R.2
Langdon, J.M.3
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27
-
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27844484013
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note
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2O, 25°C) δ (ppm): 128.79 (C-H arom); 133.16 (C arom); 162.69 (C amidine).
-
-
-
-
28
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27844467813
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note
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3); 144.31 (C-S); 161.36 (C amidine).
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-
-
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30
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27844489191
-
-
note
-
-1 (graphite monochromator). A total of 2373 reflections were collected using a Philips PW1100/16 automatic diffractometer and analyzed using the Enraf-Nonius SDP/VAX package. The raw step-scan data were converted to intensities using the Lehmann-Larsen method and corrected for Lorentz, polarization, and absorption factors. The structure was solved using MULTAN and refined to R(F) = 0.079 using 1785 reflections with I > 3σ(I). Atomic coordinates have been deposited with the Cambridge Crystallographic Data Centre and can be obtained on request to the CCDC, Union Road, Cambridge CB2 IEZ, UK. Structure factors and thermal parameters have been deposited with the British Library, Document Supply Centre at Boston Spa, Wetherby, West Yorkshire, LS23 7BQ UK, as supplementary publication No. = SUP 90449 and are available on request from the Document Supply Centre.
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