A short and efficient stereoselective synthesis of the polyhydroxylated macrolactone (+)-aspicilin

Organic Letters

Volumn 2, Issue 2, 2000, Pages 123-125

  Dixon, Darren J ^a   Foster, Alison C ^a   Ley, Steven V ^a  

^a UNIVERSITY OF CAMBRIDGE   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001166918     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol991214s     Document Type: Article

References (13)

1. Barlow, J. A.; Dixon, D. J.; Foster, A. C.; Ley, S. V.; Reynolds, D. J. J. Chem. Soc., Perkin Trans, 1 1999, 1627-1629.
2. Dixon, D. J.; Foster, A. C.; Ley, S. V.; Reynolds, D. J. J. Chem. Soc., Perkin Trans. 1 1999, 1631-1633.
3. Dixon, D. J.; Foster, A. C.; Ley, S. V.; Reynolds, D. J. J. Chem. Soc., Perkin Trans, 1 1999, 1635-1637.
4. Feige, G. B.; Lumbsch, H. T.; Huneck, S.; Elix, J. A. J. Chromatogr. 1993, 646, 417-427.
5. Booth, P. M.; Fox, C. M. J.; Ley, S. V. J. Chem. Soc., Perkin Trans. 1 1987, 121-129.
6. A similar approach was published during the course of our investigations: Nishioka, T.; Iwabuchi, Y.; Irie, H.; Hatakeyama, S. Tetrahedron Lett. 1998, 39, 5597-5600.
7. Yields for the epimer synthesis given in parentheses.
8. Narasaka, K.; Sakakura, T.; Uchimaru, T.; Guedin-Kieng, D. J. Am. Chem. Soc. 1984, 106, 2954-2961.
9. Blanchette, M. A.; Choy, W.; Davis, J. T.; Essenfeld, A. P.; Masamune, S.; Roush, W. R.; Sakai, T. Tetrahedron Lett. 1984, 25, 2183-2186.
10. Grubbs, R. H.; Chang, S. Tetrahedron 1998, 54, 4413-4450.
11. Purchased from Strem Chemicals.
12. Kobayashi, Y.; Nakano, M.; Kumar, G. B.; Kishihara, K. J. Org. Chem. 1998, 63, 7505-7515.
13. Kindly donated by Professor Hatakeyama.