Determination of lignin content of Eucalyptus globulus wood using FTIR spectroscopy

Holzforschung

Volumn 52, Issue 1, 1998, Pages 46-50

  Rodrigues, José ^a   Faix, Oskar ^b   Pereira, Helena ^c  

^a INSTITUTO DE INVESTIGAÇÃO CIENTÍFICA TROPICAL   (Portugal)

^b Federal Research Centre for Forestry and Forest Products   (Germany)

^c INSTITUTO SUPERIOR DE AGRONOMIA   (Portugal)

Author keywords

Acetyl bromide method; Calibration; Eucalyptus globulus; FTIR; Lignin content; Validation

Indexed keywords

EUCALYPTUS; EUCALYPTUS GLOBULUS;

EID: 0001153291     PISSN: 00183830     EISSN: None     Source Type: Journal    
DOI: 10.1515/hfsg.1998.52.1.46     Document Type: Article

References (26)

1. Almeida, M., H. Pereira, I. Miranda and M. Tomé. 1995. Provenance trials of Eucalyptus globulus Labill. in Portugal. In: Eucalypt plantations: Improving fibre yield and quality. Eds. B.M. Potts, N. Borralho, J.B. Reid, R.N. Crommer, W.N. Tibbits, C.A. Raymond. CRCTHF - IUFRO, Hobart, Australia, pp. 195-198.
2. Backa, S. and A. Brolin. 1991. Determination of pulp characteristics by diffuse reflectance FTIR. Tappi J. 74, 218-226.
3. Berben, S., J. Rademacher. L. Sell and D. Easty. 1987. Estimation of lignin in wood pulp by diffuse reflectance Fourier-transform infrared spectrometry. Tappi J. 70, 129-133.
4. Collier, W., T. Schultz, and V. Kalasinsky. 1992. Infrared study of lignin: reexamination of aryl-alkyl ether C-O stretching peak assignments. Holzforschung 46, 523-528.
5. Faix, O. 1992. Fourier transform infrared spectroscopy in solid state. In: Methods in Lignin Chemistry. Eds. S. Lin, C. Dence. Springer. Berlin, pp. 83-109.
6. Faix, O. and J. Böttcher. 1992. The influence of particle size and concentration in transmission and diffuse reflectance spectros-copy of wood. Holz Roh- Werkstoff 50, 221-226.
7. Faix, O., H. Schubert and R. Patt. 1989. Continuous process control of pulping by FTIR spectroscopy. International Symposium on wood and pulping chemistry. May 22-25. Raleigh, pp. 1-8.
8. Grandmaison, J., J. Thibault, S. Kaliaguine and P. Chantai. 1987. Fourier transform infrared spectrometry and thermogravimetry of partially converted lignocellulosic materials. Anal. Chem. 59, 2153-2157.
9. Hergert, H. 1971. Infrared spectra. In: Lignins: Occurrence, Formation, Structure and Function. Eds. K. Sarkanen, C. Ludwig. Wiley Interscience, New York. pp. 267-297.
10. Iiyama, K. and A. Wallis. 1988. An improved acetyl bromide procedure for determining lignin in woods and wood pulps. Wood Sci. Technol. 22, 271-280.
11. Karklin, V., A. Treimanis and V. Gromov. 1975a. Infrared spectroscopy of wood and its main components . VI. Determination of lignin in sulfate pulp samples according to ir spectra. Khim. Drev. 2, 45-52. (Chem. Abst. 83: 44945e, 1975).
12. Karklin, V., A. Treimanis and V. Gromov. 1975a. Infrared spectroscopy of wood and its main components . VI. Determination of lignin in sulfate pulp samples according to ir spectra. Khim. Drev. 2, 45-52. (Chem. Abst. 83: 44945e, 1975).
13. Karklin, V., Z. Kreicberga and M. Ekabsone. 1975b. Infrared spectroscopy of wood and its main components . VII. Use of ir-spectra to determine lignin in samples of birch wood destroyed by the fungus Fomitopsis pinicola. Khim. Drev. 2, 53-57. (Chem. Abst. 83: 44946f, 1975).
14. Karklin, V., Z. Kreicberga and M. Ekabsone. 1975b. Infrared spectroscopy of wood and its main components . VII. Use of ir-spectra to determine lignin in samples of birch wood destroyed by the fungus Fomitopsis pinicola. Khim. Drev. 2, 53-57. (Chem. Abst. 83: 44946f, 1975).
15. Karklin, V., L. Belkova, V. Gromov and J. Eidus. 1977. IR spectroscopy of wood and its main components . XIII. Determination of lignin content in nitric acid pulp preparation by ir-spectroscopy. Khim. Drev. 4, 91-96. (Chem. Abst. 87: 169420u, 1977).
16. Karklin, V., L. Belkova, V. Gromov and J. Eidus. 1977. IR spectroscopy of wood and its main components . XIII. Determination of lignin content in nitric acid pulp preparation by ir-spectroscopy. Khim. Drev. 4, 91-96. (Chem. Abst. 87: 169420u, 1977).
17. Kolboe, S. and O. Ellefsen. 1962. Infrared investigations of lignin. A discussion of some recent results. Tappi J. 45, 163-166.
18. Marton, J. and H. Sparks. 1967. Determination of lignin in pulp and paper by infrared multiple internal reflectance. Tappi J. 50, 363-368.
19. Michell, A., A. Watson and H. Higgins. 1965. An infrared spectroscopic study of delignification of Eucalyptus regnans. Tappi J. 48, 520-532.
20. Montgomery, D. and E. Peck. 1982. Introduction to linear regression analysis. Wiley-Interscience, New York. pp. 8-57.
21. Pereira, H. 1988. Variability in the chemical composition of plantation eucalypts (Eucalyptus globulus Labill.). Wood Fiber Sci. 20, 82-90.
22. Saad, S., R. Issa and M. Fahmy. 1980. Infrared spectroscopy study of bagasse and unbleached high-yield soda bagasse pulps. Holzforschung 34, 218-222.
23. Schultz, T. and D. Burns. 1990. Rapid secondary analysis of lignocellulose: comparison of near infrared (NIR) and Fourier transform infrared (FTIR). Tappi J. 73, 209-212.
24. Schultz, T., M. Templeton and G. McGinnis. 1985. Rapid determination of lignocellulose by diffuse reflectance Fourier transform infrared spectrometry. Anal. Chem. 57, 2867-2869.
25. Zhbankov, R., N. Garbuz, F. Derbentzev and V. Krotkevich. 1966. Determination of lignin in chemical and semichemical pulp by infrared spectroscopy . Zh. Prikl. Spektroskopii, Akad. Nauk. Belorussk. SSR. 4, 442-445. (Chem. Abst. 65: 12402h, 1966).
26. Zhbankov, R., N. Garbuz, F. Derbentzev and V. Krotkevich. 1966. Determination of lignin in chemical and semichemical pulp by infrared spectroscopy . Zh. Prikl. Spektroskopii, Akad. Nauk. Belorussk. SSR. 4, 442-445. (Chem. Abst. 65: 12402h, 1966).