High-pressure synthesis of [Ru2(μ-dppm)2 (μ-CO)(CO)4, Ru2(μ-dppm)(μ-dmpm) (μ-CO)(CO)4], and [Ru(dcypm)(CO)3] from Ru3(CO)12 and the diphosphines: R2PCH2PR2; R = CH3(dmpm), C6H5 (dppm) and C6H11 (dcypm).

Polyhedron

Volumn 16, Issue 9, 1997, Pages 1453-1459

  Ferrence, Gregory M ^a,b   Fanwick, Phillip E ^a   Kubiak, Clifford P ^a   Haines, Raymond J ^c  

^a PURDUE UNIVERSITY   (United States)

^b AMHERST COLLEGE   (United States)

^c UNIVERSITY OF KWAZULU NATAL   (South Africa)

Author keywords

Complex; diphosphine; Crystal structure; Dinuclear ruthenium; High pressure synthesis

Indexed keywords

EID: 0001148218     PISSN: 02775387     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0277-5387(96)00450-0     Document Type: Article

References (24)

1. Field, J. S., Haines, R. J., Stewart, M. W., Sundermeyer, J. and Woollam, S. F., J. Chem, Soc., Dalton Trans. 1993, 947.
2. Field, J. S., Haines, R. J., Honrath, U., Sundermeyer, J. and Woollam, S. F. J. Organomet. Chem. 1990, 395, C9.
3. Engel, D. W., Field, J. S., Haines, R. J., Honrath, U., Horsfield, E. C., Sundermeyer, J. and Woollam, S. F., J. Chem. Soc., Dalton Trans. 1994, 1131.
4. Field, J. S., Francis, A. M. A. and Haines, R. J., J. Organomet. Chem. 1988, 356, C23.
5. Leeuw, G. D., Field, J. S., Haines, R. J., McCulloch, B., Meintjies, E., Monberg, C., Oliver, G. M., Ramdial, P., Sampson, C. N., Sigwarth, B., Steen, N. D. and Moodley, K. G., J. Organomet. Chem. 1984, 275, 99.
6. Haines, R. J., Comprehensive Organometallic Chemistry II, Vol. 7, eds in chief E. W. Abel, F. G. A. Stone and G. Wilkinson, 1995, pp. 625-68, Pergamon, Oxford.
7. Johnson, K. A. and Gladfelter, W. L., Organometallics, 1989, 8, 2866.
8. Engel, D. W., Moodley, K. G., Subramony, L. and Haines, R. J., J. Organomet. Chem. 1988, 349, 393.
9. Mirza, H. A., Vittal, J. J. and Puddephatt, R. J., Inorg. Chem. 1993, 32, 1327.
10. Johnson, K. A. and Gladfelter, W. L., Organometallics, 1990, 9, 2101.
11. Granger, R. M., Fanwick, P. E., Haines, R. J. and Kubiak, C. P., Inorg. Chem. 1993, 32, 3570.
12. Walker, N. and Stuart, D., Acta Cryst. 1983, A39, 158.
13. Sheldrick, G. M., Institut für Anorganische Chemie der Universitat Gottingen, Germany, 1986.
14. Killean, R. C. G. and Lawrence, J. L., Acta Cryst. 1969, B25, 1750.
15. Cromer, D. T. and Waber, J. T., International Tables for X-Ray Crystallography Vol. IV. Table 2.2B. Kynoch Press, Birmingham (1974).
16. Ibers, J. A. and Hamilton, W. C., Acta Cryst. 1964, 17, 781.
17. Cromer, D. T., International Tables for X-Ray Crystallography, Vol. IV. Table 2.3.1. Kynoch Press, Birmingham (1974).
18. Fair, C. K., MolEN Structure Determination System, Delft Instruments, Delft, The Netherlands (1990).
19. Johnson, C. K., ORTEPII, Report ORNL-5138, Oak Ridge National Laboratory, Tennessee, USA (1976).
20. Morgan, C. A., Fanwick, P. E. and Rothwell, I. P., Inorg. Chim. Acta, 1994, 224, 105.
21. Sanchez-Delgado, R. A., Bradley, J. S. and Wilkinson, G., J. Chem. Soc., Dalton Trans. 1976, 339.
22. Dahan, F., Sabo, S. and Chaudret, B., Acta Cryst. 1984, C40, 786.
23. Jones, R. A., Wilkinson, G., Galas, A. M. R., Hursthouse, M. B. and Malik, K. M. A., J. Chem. Soc., Dalton Trans. 1980, 1771.
24. Garrou, P. E., Chem. Rev. 1981, 81, 229.