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84891518417
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12SH-derivatized Au nanoparticles of 20 Å [6 b] in diameter.
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36449006440
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84891546026
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2 and all-trans extended chain length is 29.8 Å would provide an area per chain end that is 14-fold greater.
-
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16
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84891535523
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-
note
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3) leads to a disordering or solubilization of the chains on the particle. This is evident in solution-state NMR studies, where the spectra become relatively well-resolved and narrow-lined, indicative of a highly mobile state. Any solvent which allows the isolation of the RS-Au particles in solution will most likely also solvate the alkyl chains and disrupt chain-chain interactions; the net result is an absence of any phase-transition behavior in the temperature region probed in Figures 3 and 4.
-
-
-
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17
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84891547265
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note
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Temperature-programmed desorption studies of a hexdacanethiol monolayer chemisorbed on a Au(111) single-crystal surface show that desorption of the thiol occurs at T≥227°C [15 a].
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