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For recent reviews, see: Hashimoto, S.; Ikegami, S. Pharmacia 1991, 27, 50; Toshima, K.; Tatsuta, K. Chem. Rev. 1993, 93, 1503; Schmidt, R.R. Comprehensive Organic Synthesis, Pergamon Press: Oxford, 1991; Vol.6, p 33; Sinaÿ, P. Pure Appl. Chem. 1991, 63, 519; Suzuki, K.; Nagasawa, T. J. Synth. Org. Chem. Jpn. 1992, 50,378; Ito, Y.; Ogawa, Jikkenkagakukoza; Maruzen: Tokyo, 1992, Vol.26, p 267; Banoub, J., Boullanger, P. and Lafont, D. Chem. Rev. 1992, 92, 1167; Schmidt, R. R. Carbohydrates, Synthetic Methods and Applications in Medicinal Chemistry; Kodansha: Tokyo, 1992; p 66.
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17
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1542615632
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note
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4) and concentrated in vacuo. The residue was purified by column chromatography on silica gel (9 : 1 hexane : EtOAc).
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