Synthesis and characterization of yttrium complexes containing a tridentate linked amido-cyclopentadienyl ligand

Organometallics

Volumn 17, Issue 3, 1998, Pages 485-488

  Hultzsch, Kai C ^a   Spaniol, Thomas P ^a   Okuda, Jun ^a  

^a JOHANNES GUTENBERG UNIVERSITY   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001097377     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om970701d     Document Type: Article

References (41)

1. (a) Schaverien, C. J. Adv. Organomet. Chem. 1994, 36, 283.
2. (b) Edelmann, F. T. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon Press: Oxford, 1995; Vol. 4, Chapter 2.
3. (c) Schumann, H.; Meese-Marktscheffel, J. A.; Esser, L. Chem. Rev. 1995, 95, 865.
4. (d) Piers, W. E.; Shapiro, P. J.; Bunel, E. E.; Bercaw, J. E. Synlett 1990, 74.
5. (a) Manastyrskyj, S.; Maginn, R. E.; Dubeck, M. Inorg. Chem. 1963, 2, 904.
6. (b) Jamerson, J. D.; Masino, A. P.; Takats, J. J. Organomet. Chem. 1974, 65, C33.
7. (c) Schumann, H.; Albrecht, I.; Pickardt, J.; Hahn, E. J. Organomet. Chem. 1984, 276, C5.
8. (d) Albrecht, I.; Hahn, E.; Pickardt, J.; Schumann, H. Inorg. Chirn. Acta 1985, 110, 145.
9. (e) Albrecht, I.; Schumann, H. J. Organomet. Chem. 1986, 310, C29.
10. (f) Hazin, P. N.; Huffman, J. C.; Bruno, J. W. Organornetallics 1987, 6, 23.
11. (g) Schumann, H.; Albrecht, I.; Gallagher, M.; Hahn, E.; Janiak, C.; Kolax, C.; Loebel, J.; Nickel, S.; Palamidis, E. Polyhedron 1988, 7, 2307.
12. (h) van der Heijden, H.; Pasman, P.; de Boer, E. J. M.; Schaverien, C. J.; Orpen, A. G. Organometallics 1989, 8, 1459.
13. (i) Zhou, X.; Wu, Z.; Ma, H.; Xu, Z.; You, X. Polyhedron 1994, 13, 375.
14. (a) Heeres, H. J.; Meetsma, A.; Teuben, J. H,; Rogers, R. D. Organometallics 1989, 8, 2637.
15. (b) Schaverien, C. J.; Frijns, J. H. G.; Heeres, H. J.; van den Hende, J. R.; Teuben, J. H.; Spek, A. L. J. Chem. Soc., Chem. Commun. 1991, 642.
16. (c) Schaverien, C. J. Organometallics 1994, 13, 69.
17. Schumann, H.; Meese-Marktscheffel, J. A.; Dietrich, A. J. Organomet. Chem. 1989, 377, C5.
18. Piers, W. E.; Bunel, E. E.; Bercaw, J. E. J. Organomet. Chem. 1991, 407, 51.
19. (a) Shapiro, P. J.; Bunel, E.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1990, 9, 867.
20. (b) Shapiro, P. J.; Cotter, W. D.; Schaefer, W. P.; Labinger, J. A.; Bercaw, J. E. J. Am. Chem. Soc. 1994, 116, 4623.
21. (a) Mu, Y.; Piers, W. E.; MacDonald, M.-A.; Zaworotko, M. J. Can. J. Chem. 1995, 73, 2233.
22. (b) Mu, Y.; Piers, W. E.; MacQuarrie, D. C.; Zaworotko, M. J.; Young, V. G., Jr. Organometallics 1996, 15, 2720.
23. du Plooy, K. E.; Moll, U.; Wocadlo, S.; Massa, W.; Okuda, J. Organometallics 1995, 14, 3129.
24. (a) Hultzsch, K. C. Diploma Thesis, University of Mainz, Germany, 1996.
25. (b) Hultzsch, K. C.; Spaniol, T. P.; Okuda, J. Organometallics 1997, 16, 4845.
26. (c) Hultzsch, K. C.; Okuda, J. Macromol. Rapid Commun. 1997, 18, 809.
27. 2 (Ln = Y, Lu) with bridging lithium atoms, see: Hogerheide, M. P.; Grove, D. M.; Boersma, J.; Jastrzebski, J. T. B. H.; Kooijman, H.; Spek, A. L.; van Koten, G. Chem. Eur. J. 1995, 1, 343.
28. 2 (see ref 10), one might expect to find three molecules of THF in 1, one coordinated to yttrium and two to lithium.
29. (a) Booij, M.; Kiers, N. H.; Heeres, H. J.; Teuben, J. H. J. Organomet. Chem. 1989, 364, 79.
30. (b) Booij, M.; Kiers, N. H.; Meetsma, A.; Teuben, J. H. Organometallics 1989, 8, 2454.
31. Booij, M.; Deelman, B.-J.; Duchateau, R.; Postma, D. S.; Meetsma, A.; Teuben, J. H. Organometallics 1993, 12, 3531.
32. Zsolnai, L.; Pritzkow, H. ZORTEP Ortep Program for PC; Universität Heidelberg: Heidelberg, Germany, 1994.
33. Cent-Y = 2.367(3) Å, see ref 12b.
34. Cent-Y = 2.392(3) Å, see Duchateau, R.; Meetsma, A.; Teuben, J. H. Organometallics 1996, 15, 1656.
35. Cent-Y = 2.415 Å, see Evans, W. J.; Boyle, T. J.; Ziller, J. W. Organometallics 1993, 12, 3998.
36. Rausch, M. D.; Foust, D. F.; Rogers, R. D.; Atwood, J. L. J. Organomet. Chem. 1984, 265, 241.
37. den Haan, K. H.; de Boer, J. L.; Teuben, J. H.; Spek, A. L.; Kojic-Prodic, B.; Hays, G. R.; Huis, R. Organometallics 1986, 5, 1726.
38. 1H NMR spectrum.
39. (a) Fair, C. K. MolEN, An Interactive Structure Solution Procedure: Enraf-Nonius, Delft: The Netherlands, 1990.
40. (b) Sheldrick, G. M. SHELXL-93, Program for the Refinement of Crystal Structures; University of Göttingen: Göttingen, Germany, 1993.
41. (c) Sheldrick, G. M. SHELXS-86, Program for the Solution of Crystal Structures; University of Göttingen: Göttingen, Germany, 1986.