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85033816655
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For a discussion of these problems, see ref 2a, pp 152-3, and ref 2c, p 4.
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8
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3 upon heating, liberating volatile titanium complexes instead: Kessler, V. G.; Hubert-Pfalzgraf, L. G.; Daniele, S.; Gleizes, A. Chem. Mater. 1994, 6, 2336.
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22
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85033814487
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note
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-1, KBr) 3600-3000 s, br; 2935 m; 2866 m; 2824 m; 2653 m; 2534 m; 1967 w; 1928 w; 1638 m, br; 1454 m, br; 1379 m, 1355 m; 1335 m; 1236 m; 1222 m; 1119 sh; 1085 s; 1050 s; 911 m; 880 s; 818 m; 601 s; 530 sh; 512 s; 453 s.
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-
-
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23
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85033811565
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note
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2, is obtained when Ba metal and titanium isopropoxide are used as reactants and the preparation is carried out in a dry nitrogen atmosphere.
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-
-
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24
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85033827588
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note
-
40) were located from a difference Fourier and refined as independent isotropic atoms. Methylene hydrogen atoms on the ordered glycol and glycolate ligands were included in the structural model at fixed idealized tetrahedral positions with a C-H bond length of 0.96 Å and an isotropic thermal parameter 20% greater than the equivalent isotropic thermal parameter of the carbon atom to which it is bonded.
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25
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0001020648
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(a) Day, V. W.; Eberspacher, T. A ; Klemperer, W. G.; R. Planalp, P.; Schiller, P. W.; Yagasaki, A.; Zhong, B. Inorg. Chem. 1993, 32, 1629.
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R. Planalp, P.4
Schiller, P.W.5
Yagasaki, A.6
Zhong, B.7
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26
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0000088580
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(b) Besecker, C. J.; Day, V. W.; Klemperer, W. G.; Thompson, M. R. J. Am. Chem. Soc. 1984, 106, 4125
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Thompson, M.R.4
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27
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85033826002
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note
-
The first number in parentheses following an average value of a bond length or angle is the root-mean-square estimated standard deviation of an individual datum. The second and third numbers are the average and maximum deviations from the average value, respectively. The fourth number represents the number of individual measurements which are included in the average value.
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29
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0001268395
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(a) Naka, S.; Nakakita, F.; Suwa, Y.; Inagaki, M. Bull. Chem. Soc. Jpn. 1974, 47, 1168.
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30
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85033821741
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Powder Diffraction File Card No. 31-0174. Joint Committee on Powder Diffraction Standards, 1994
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(b) Powder Diffraction File Card No. 31-0174. Joint Committee on Powder Diffraction Standards, 1994.
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31
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85033814234
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Powder Diffraction File Card No. 5-626. Joint Committee on Powder Diffraction Standards, 1993
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Powder Diffraction File Card No. 5-626. Joint Committee on Powder Diffraction Standards, 1993.
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32
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0004217652
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