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2O. TEOS was added to the surfactant in the water:ethanol-mixed solvent under rapid stirring for 30 min, and then the mixture was heated at 100°C in an autoclave for 48 hours under static condition. The product was filtered, washed with cold ethanol, and air-dried. Finally, the surfactant was removed from the surfactant-containing product by calcination in air at 650°C for 4 hours or by extraction with hot ethanol.
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This research was supported by NSF through Chemistry Research Group grant CHE-9633798
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This research was supported by NSF through Chemistry Research Group grant CHE-9633798.
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