Metal core rearrangements in hetero-bimetallic nona-osmium carbonyl clusters; the crystal and molecular structures of [Os9(CO)24{Au(PCy3i)}2] and [Os9(CO)23(Au2DPPE)]

Journal of Organometallic Chemistry

Volumn 550, Issue 1-2, 1998, Pages 131-139

  Akhter, Zareen ^a   Ingham, Scott L ^a   Lewis, Jack ^a   Raithby, Paul R ^a  

^a Department of Chemistry ^*  (United Kingdom)

Author keywords

Cluster carbonyls; Gold; Osmium; Phosphines; X ray structure

Indexed keywords

STAPHYLOCOCCUS PHAGE 3A;

EID: 0001010157     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(97)00188-5     Document Type: Article

References (26)

1. (a) E. Charalambous, L.H. Gade, B.F.G. Johnson, T. Kotch, A.J. Lees, J. Lewis, M. McPartlin, Angew. Chem. Int. Ed. Engl. 29 (1990) 1137.
2. (b) L.H. Gade, B.F.G. Johnson, J. Lewis, M. McPartlin, T. Kotch, A.J. Lees, J. Am. Chem. Soc. 113 (1991) 8698.
3. (a) L.H. Gade, B.F.G. Johnson, J. Lewis, M. McPartlin, H.R. Powell, J. Chem. Soc. Chem. Commun. (1990) 110.
4. (b) R. Della Pergola, F. Demartin, L. Garlaschelli, M. Manassero, S. Martinengo, N. Masciocchi, M. Sansoni, Organometallics 10 (1991) 2239.
5. (c) A.J. Whoolery, L.F. Dahl, J. Am. Chem. Soc. 113 (1991) 6683.
6. (d) A. Fumagalli, S. Martinengo, V.G. Albano, D. Braga, F. Grepioni, J. Chem. Soc. Dalton Trans. (1993) 2047.
7. (e) V. Dearing, S.R. Drake, B.F.G. Johnson, J. Lewis, M. McPartlin, H.R. Powell, J. Chem. Soc. Chem. Commun. (1988) 1331.
8. (a) L.H. Gade, B.F.G. Johnson, J. Lewis, M. McPartlin, H.R. Powell, J. Chem. Soc. Chem. Commun. (1992) 921.
9. (b) L.H. Gade, Angew. Chem. Int. Ed. Engl. 32 (1993) 24.
10. (c) J.W. Lauher, K. Wald, J. Am. Chem. Soc. 103 (1981) 7648.
11. (d) L.W. Bateman, M. Green, J.A.K. Howard, K.A. Mead, R.M. Mills, I.D. Salter, F.G.A. Stone, P. Woodward, J. Chem. Soc. Chem. Commun. (1982) 773.
12. (a) S.L. Ingham, J. Lewis, P.R. Raithby, J. Chem. Soc. Chem. Commun. (1993) 166.
13. (b) Z. Akhter, S.L. Ingham, J. Lewis, P.R. Raithby, Angew. Chem. Int. Ed. Engl. 35 (1996) 992.
14. (c) A.J. Amoroso, L.H. Gade, B.F.G. Johnson, J. Lewis, P.R. Raithby, W.-T. Wong, Angew. Chem. Int. Ed. Engl. 30 (1991) 107.
15. Z. Akhter, S.L. Ingham, J. Lewis, P.R. Raithby, J. Organomet. Chem. 474 (1994) 165.
16. A.J. Amoroso, B.F.G. Johnson, J. Lewis, P.R. Raithby, W.-T. Wong, J. Chem. Soc. Chem. Commun. (1991) 814.
17. B.F.G. Johnson, J. Lewis, W.J.H. Nelson, P.R. Raithby, M.D. Vargas, J. Chem. Soc. Chem. Commun. (1983) 608.
18. D.M.P. Mingos, J. Cherm. Soc. Chem. Commun. (1983) 706.
19. D.F. Shriver, Manipulation of Air-Sensitive Compounds, McGraw-Hill, New York, 1969.
20. A.M. Mueting, B.D. Alexander, P.D. Bole, A.L. Casalnuovo, L.N. Itp, B.J. Johnson, L.H. Pignolet, Inorg. Synth. 29 (1992) 280.
21. S.J. Berners-Price, M.A. Mazid, P.J. Sadler, J. Chem. Soc. Dalton Trans. (1984) 969.
22. N. Walker, D. Stuart, Acta Crystallogr. Sect. A: 39 (1983) 158.
23. H.D. Flack, Acta Crystallogr. Sect. A: 39 (1983) 876.
24. TEXSAN: Single Crystal Structure Analysis Software, Version 1.6, 1993, Molecular Structure Corporation, The Woodlands, TX 77381, USA.
25. G.M. Sheldrick, Acta Crystallogr. Sect. A: 46 (1993) 467.
26. G.M. Sheldrick, SHELXL-93, Program for Structure Refinement, University of Göttingen, 1993.