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The crystal was immersed in a lube-oil additive, which allowed for manipulation on the bench top and prevented decomposition due to air or moisture. The crystal was secured to a glass fiber (the oil acts as the adhesive) which was attached to an elongated brass mounting pin. Further details appear in: Hope, H. Experimental Organometallic Chemistry: A Practicum in Synthesis and Characterization; Wayda, A. L., Darensbourg, M. Y., Eds.; ACS Symposium Series 357; American Chemical Society: Washington, DC, 1987.
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33845282603
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For a related example, see: Evans. W. J.; Drummond, D. K.; Grate, J. W.; Zhang, H.; Atwood, J. L. J. Am. Chem. Soc. 1987, 109, 3928.
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and references therein
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2542444417
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Several attempts were made to obtain precise metrical data for crystals of 7, but the data were not of sufficient quality to yield any information other than atom connectivity
-
Several attempts were made to obtain precise metrical data for crystals of 7, but the data were not of sufficient quality to yield any information other than atom connectivity.
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53
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