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Only one diastereomer of alcohol 4 was observed by 'H and 13C NMR. The absolute configuration was determined from the 'H NMR 6 Hz coupling constant between the two ring protons of an oxazolidinone derivative as previously described. (Williams, T. M.; Crumble, R.; Mosher, H. S. J. Org. Chem. 1985, 50, 91-97.) In the case of trityl-protected amine, the best observed diastereomeric ratio was only 2:1
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note
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1H NMR.
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