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0344785165
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A butatrienylidene six electron donor ligand in a cluster compound has also been reported: Adams, C. J.; Bruce, M. I.; Skelton, B. W.; White, A. H. J. Chem. Soc., Chem. Commun. 1996, 2663.
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0002581706
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32
-
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5244290515
-
-
note
-
5Ru: C, 60.85; H, 5.43; N, 1.13. Found: C, 60.57; H, 5.24; N, 1.12.
-
-
-
-
33
-
-
5244321709
-
-
note
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2, which could not be localized or considered as disordered or partially occupied. The packing diagram reveals tubular channels formed by the hydrophobic phenyl rings of the dppm ligands. We assume that the solvent resides in these channels.
-
-
-
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34
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0004082223
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Universiät Göttingen, Göttingen, Germany
-
Sheldrick, G. M. Program SHELXL93, Universiät Göttingen, Göttingen, Germany, 1993.
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(1993)
Program SHELXL93
-
-
Sheldrick, G.M.1
-
35
-
-
5244308952
-
-
note
-
5Ru: C, 59.78; H, 4.84; N, 1.18. Found: C, 59.05; H, 4.82; N, 1.21.
-
-
-
-
36
-
-
5244273649
-
-
note
-
2: C, 40.65; H, 7.17; N, 1.61. Found: C, 40.84; H, 6.94; N, 1.59.
-
-
-
-
37
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84985741234
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-
(a) Duetsch, M.; Stein, F.; Lackmann, R.; Pohl, E.; Herbst-Irmer, R.; de Meijere, A. Chem. Ber. 1992, 125, 2051.
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Duetsch, M.1
Stein, F.2
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Pohl, E.4
Herbst-Irmer, R.5
De Meijere, A.6
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38
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4243136860
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(b) Stein, F.; Duetsch, M.; Pohl, E.; Herbst-Irmer, R.; de Meijere, A. Organometallics 1993, 12 2556
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Stein, F.1
Duetsch, M.2
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Herbst-Irmer, R.4
De Meijere, A.5
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39
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0344352453
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Fischer, E. O.; Kalder, H. J.; Frank, A.; Köhler, F. H.; Huttner, G. Angew. Chem., Int. Ed. Engl. 1976, 33, 1360.
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Fischer, E.O.1
Kalder, H.J.2
Frank, A.3
Köhler, F.H.4
Huttner, G.5
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42
-
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5244375445
-
-
note
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2 (SHELXL93). With the exception of the solvent carbon atoms, all non-H atoms were refined with anisotropic thermal parameters. One phenyl ring (ratio 0.501(0.009)/0.499(0.009)), C10 (0.54(0.02)70.46(0.02)), C3x, C4-C7 (0.578(0.009)/0.422(0.009)) of the carbon chain and one solvent molecule (0.75(0.02)/0.25(0.02)) were found to be disordered; an additional solvent molecule was refined as "half-occupied". All hydrogen atoms were introduced at their geometric positions and treated according to the "riding model". Atomic coordinates, bond lengths and angles, and thermal parameters of 3a and 4a have been deposited at the Cambridge Crystallographic Data Centre, University Chemical Laboratory, Lens-field Road, Cambridge CB2 1EZ, UK (deposition no. CCDC-100-155).
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