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Volumn 35, Issue 4, 1996, Pages 943-948

Synthesis and Structure of [TpBut2]In, a Highly Twisted [Tris(3,5-di-tert-butylpyrazolyl)hydroborato]indium(I) Complex: Comparison with the Re-Evaluated Ordered Structure of [TBut]In

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EID: 0000931111     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic9509948     Document Type: Article
Times cited : (38)

References (44)
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    • note
    • 1a Thus, the tris(pyrazolyl)hydroborato ligands are represented by the abbreviation Tp, with the 3- and 5-alkyl substituents listed respectively as superscripts.
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    • For some leading references, see: (a) Marsh, R. E.; Bernai, I. Acta Crystallogr. 1995, B51, 300-307. (b) Marsh, R. E. Acta Crystallogr. 1994, A50, 450-455. (c) Marsh, R. E.; Herbstein, F. H. Acta Crystallogr. 1988, B44, 77-78. (d) Marsh, R. E.; Herbstein, F. H. Acta Crystallogr. 1983, B39, 280-287. (e) Marsh, R. E.; Schomaker, V. Inorg. Chem. 1979, 18, 2331-2336. (f) Marsh, R E. Acta Crystallogr. 1986, B42, 193-198. (g) Marsh, R. E. Acta Crystallogr. 1981, B37, 1985-1988. (h) Marsh, R. E. Inorg. Chim. Acta 1989, 157, 1-2. (i) Baur, W. H.; Tillmanns, E. Acta Crystallogr. 1986, B42, 95-111.
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    • The structure was also attempted in Ama2, but similar, and more extreme, problems were encountered compared to those for Cmcm
    • The structure was also attempted in Ama2, but similar, and more extreme, problems were encountered compared to those for Cmcm.
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    • note
    • Obviously, it is plausible that small deviations from centrosymmetry may not be sufficient to prevent a strictly noncentrosymmetric structure from being refined in a centrosymmetric space group. In this specific instance, we are referring to a disorder in which there is a significant structural change.
  • 42
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    • For another example in which a structure that was initially refined in centrosymmetric P1̄ is better described as noncentrosymmetric P1, see: Calabrese, J. C.; Gardner, K. H. Acta Crystallogr. 1985, C41, 389-392.
    • (1985) Acta Crystallogr. , vol.C41 , pp. 389-392
    • Calabrese, J.C.1    Gardner, K.H.2


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