Conformationally restrained octahedral metallacrown ethers with 1,2-(Ph2P(CH2CH2O)2) 2C6H4 ligands. X-ray crystal structure of cis-Mo(CO)4{1,2-(Ph2P(CH2CH2O) 2)2C6H4-P,P′}

Organometallics

Volumn 17, Issue 16, 1998, Pages 3550-3556

  Duffey, Christina H ^a   Lake, Charles H ^b   Gray, Gary M ^b  

^a SAMFORD UNIVERSITY   (United States)

^b UNIVERSITY OF ALABAMA AT BIRMINGHAM   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000930562     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om970785q     Document Type: Article

References (29)

1. (a) Powell, J.; Kuksis, A.; May, C. J.; Nyberg, S. C.; Smith, S. J. J. Am. Chem. Soc. 1981, 103, 5941.
2. (b) Powell, J.; Nyberg, S. C.; Smith, S. J. Inorg. Chim. Acta 1983, 76, L75.
3. (c) Powell, J.; Ng, K. S.; Ng, W. W.; Nyberg, S. C. J. Organomet. Chem. 1983, 243, C1.
4. (d) Powell, J.; Gregg, M.; Kuskis, A.; Meindl, P. J. Am. Chem. Soc. 1983, 105, 1064.
5. (e) Powell, J.; Gregg, M. R.; Kuksis, A.; May, C. J.; Smith, S. J. Organometallics 1989, 8, 2918.
6. (f) Powell, J.; Kuskis, A.; May, C. J.; Meindl, P. E.; Smith, S. J. Organometallics 1989, 8, 2933.
7. (g) Powell, J.; Gregg, M. R.; Meindl, P. E. Organometallics 1989, 8, 2942.
8. (h) Powell, J.; Lough, A.; Wang, F. Organometallics 1992, 11, 2289.
9. (a) Alcock, N. W.; Brown, J. M.; Jeffery, J. C. J. Chem. Soc., Chem. Commun. 1974, 829.
10. (b) Alcock, N. W.; Brown, J. M.; Jeffery, J. C. J. Chem. Soc., Dalton Trans. 1976, 583.
11. (c) Thewissen, D. H. W.; Timmer, K.; Noltes, J. G.; Marsman, J. W.; Laine, R. M. Inorg. Chim. Acta 1985, 97, 143.
12. (d) Timmer, K.; Thewissen, H. D.; Marsman, J. W. Recl. Trav. Chim. Pays-Bas 1988, 107, 248.
13. Timmer, K.; Thewissen, D. H. W. Inorg. Chim. Acta 1985, 100, 235.
14. Varshney, A.; Gray, G. M. Inorg. Chem. 1991, 30, 1748.
15. Varshney, A.; Webster, M. L.; Gray, G. M. Inorg. Chem. 1992, 31, 2580.
16. Gray, G. M.; Duffey, C. H. Organometallics 1994, 13, 1542.
17. Gray, G. M.; Varshney, A.; Duffey, C. H. Organometallics 1995, 14, 238.
18. Gray, G. M.; Duffey, C. H. Organometallics 1995, 14, 245.
19. Gray, G. M.; Fish, F. P.; Duffey, C. H. Inorg. Chim. Acta 1996, 246, 229.
20. Ehrl, W.; Ruck, R.; Vahrenkamp, H. J. Organomet. Chem. 1973, 56, 285.
21. Duffey, C.; Gray, G. M. Acta Crystallogr. 1996, C52, 861.
22. Kopolow, T. E.; Esch, T. E. H.; Smid, J. Macromolecules 1973, 6, 133.
23. Siemens SHELXTL-PC Manual, Release 4.1; Siemens Analytical Instruments: Madison, WI, 1990.
24. Churchill, M. R. Inorg. Chem. 1973, 12, 1213.
25. Lindoy, L. F. The Chemistry of Macrocyclic Ligand Complexes; Cambridge University Press: New York, 1989.
26. Smith, D. C., Jr.; Gray, G. M. Inorg. Chem. 1998, 37, 1791.
27. Redfield, D. A.; Nelson, J. H.; Cary, L. W. Inorg. Nucl. Chem. Lett. 1974, 10, 727.
28. Duffey, C. H. Ph.D. Thesis, 1996, The University of Alabama at Birmingham, 1996.
29. Pregosin, P. S.; Kunz, R. W. NMR: Basic Principles in Progress; Springer-Verlag: Berlin, 1979.