Synthesis of the First Perfluoro-spiro-bis-crown Ethers

Journal of Organic Chemistry

Volumn 62, Issue 5, 1997, Pages 1527-1528

  Wei, Han Chao ^a   Lynch, Vincent M ^a   Lagow, Richard J ^a  

^a University of Texas at Austin   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000914773     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo961628o     Document Type: Article

References (20)

1. Lin, W. H.; Bailey, W. I.; Lagow, R. J. J. Chem. Soc., Chem. Commun. 1985, 1350.
2. (a) Clark, W. D.; Lin, T. Y.; Maleknia, S. D.; Lagow, R. J. J. Org. Chem. 1990, 55, 5933.
3. (b) Lin, T. Y.; Lagow, R. J. J. Chem. Soc., Chem. Commun. 1991, 12.
4. (c) Lin, T. Y.; Roesky, H. W.; Lagow, R. J. Synth. Commun. 1993, 23, 2451.
5. Schweighardt, F. K.; Rubertone, J. A. U.S. Patent 4,838,274, 1989.
6. (a) Brodbelt, J. S.; Maleknia, S. D.; Liou, C. C.; Lagow, R. J. J. Am. Chem. Soc. 1991, 113, 5913.
7. (b) Brodbelt, J. S.; Maleknia, S. D.; Lagow, R. J.; Lin, T. Y. J. Chem. Soc., Chem. Commun. 1991, 1705.
8. (c) Brodbelt, J. S.; Liou, C. C.; Maleknia, S. D.; Lin, T. Y.; Lagow, R. J. J. Am. Chem. Soc. 1993, 115, 11069.
9. (d) Lin, T. Y.; Lin, W. H.; Clark, W. D.; Lagow, R. J.; Larson, S. D.; Simonsen, S. H.; Lynch, V. M.; Brodbelt, J. S.; Maleknia, S. D.; Liou, C. C. J. Am. Chem. Soc. 1994, 116, 5172.
10. (a) Kimura, E.; Shionoya, M.; Okamoto, M.; Nada, H. J. Am. Chem. Soc. 1988, 110, 3679.
11. (b) Shionoya, M.; Kimura, E.; Iitaka, Y. J. Am. Chem. Soc. 1990, 112, 9237.
12. (a) We followed the simple crown ether compound nomenclature proposed by Pedersen: Pedersen, C. J. J. Am. Chem. Soc. 1967, 89, 7017. Pedersen, C. J.; Frensdorff, H. K. Angew. Chem., Int. Ed. Engl. 1972, 11, 16.
13. (a) We followed the simple crown ether compound nomenclature proposed by Pedersen: Pedersen, C. J. J. Am. Chem. Soc. 1967, 89, 7017. Pedersen, C. J.; Frensdorff, H. K. Angew. Chem., Int. Ed. Engl. 1972, 11, 16.
14. (b) For more discussion of new nomenclature of crown ether compounds see: Weber, E.; Vögtle, F. Inorg. Chim. Acta 1980, 45, L65.
15. The author has deposited atomic coordinates for this structure with the Cambridge Crystallographic Data Centre. The coordinates can be obtained, on request, from the Director, Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK.
16. Czugler, M. and Weber, E. J. Chem. Soc., Chem. Commun. 1981, 472.
17. BRAYCO 815Z perfluoropolyether oil, Castrol, Inc., Bray Products Division, Irvine, CA.
18. Bogatsky, A. V.; Lukyanenko, N. G.; Lobach, A. V.; Nazarova, N. Yu.; Karpenko, L. P. Synthesis 1984, 139.
19. Weber, E. J. Org. Chem. 1982, 47, 3478.
20. Bierschenk, T. R.; Juhlke, T. J.; Lagow, R. J.; Kawa, H. U. S. Patent 5, 093, 432, 1992.