Group 4 metal amido fluorides and chlorides: Molecular structures and the first comparison in ethylene polymerization catalysis

Organometallics

Volumn 15, Issue 14, 1996, Pages 3176-3181

  Shah, Syed A A ^a   Dorn, Hendrik ^a   Voigt, Andreas ^a   Roesky, Herbert W ^a   Parisini, Emilio ^a   Schmidt, Hans Georg ^a   Noltemeyer, Mathias ^a  

^a UNIVERSITY OF GÖTTINGEN   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000914121     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om960177v     Document Type: Article

References (56)

1. Sinn, H.; Kaminsky, W. Adv. Organomet. Chem. 1980, 18, 99.
2. Jordan, R. F. Adv. Organomet. Chem. 1991, 32, 325.
3. Marks, T. J. Acc. Chem. Res. 1992, 25, 57.
4. Horton, A. D. Trends Polym. Sci. 1994, 2, 158.
5. Kaminsky, W. Angew. Makromol. Chem. 1994, 223, 101.
6. Bochmann, M.; Lancaster, S. J. Organometallics 1993, 12, 633.
7. Hlatky, G. G.; Eckmann, R. R.; Turner, H. W. Organometallics 1992, 11, 1413.
8. Herrmann, W. A.; Anwander, R.; Riepl, H.; Scherer, W.; Whitaker, C. R. Organometallics 1993, 12, 4342.
9. Tsai, W.-M.; Chien, J. C. W. J. Polym. Sci., A: Polym. Chem. 1994, 32, 149.
10. Möhring, P. C.; Coville, N. C. J. Organomet. Chem. 1994, 479, 1.
11. Spaleck, W.; Küber, F.; Winter, A.; Rohrmann, J.; Bachmann, B.; Antberg, M.; Dolle, V.; Paulus, E. F. Organometallics 1994, 13, 954.
12. Brintzinger, H.-H.; Fischer, D.; Mülhaupt, R.; Rieger, B.; Waymouth, R. Angew. Chem. 1995, 107, 1255; Angew. Chem. Int. Ed. Engl. 1995, 34, 1143 and references cited therein.
13. Brintzinger, H.-H.; Fischer, D.; Mülhaupt, R.; Rieger, B.; Waymouth, R. Angew. Chem. 1995, 107, 1255; Angew. Chem. Int. Ed. Engl. 1995, 34, 1143 and references cited therein.
14. (a) Canich, J. A. M. Eur. Pat. Appl. 420 436, 1991.
15. (b) Canich, J. A. M.; Hlatky, G. G.; Turner, H. W. U.S. Patent 542 236, 1990.
16. (c) Campbell, R. E. U.S. Patent 5 066 741, 1991.
17. (d) LaPointe, R. E.; Rosen, R. K.; Nickias, P. N. Eur. Pat. 495 375, 1992.
18. Shapiro, P. J.; Bunel, E.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1990, 9, 867.
19. Okuda, J. Chem. Ber. 1990, 123, 1649.
20. (a) Herrmann, W. A.; Morawietz, M. J. A.; Priermeier, T. Angew. Chem. 1994, 106, 2025; Angew. Chem., Int. Ed. Engl. 1994, 33, 1941.
21. (a) Herrmann, W. A.; Morawietz, M. J. A.; Priermeier, T. Angew. Chem. 1994, 106, 2025; Angew. Chem., Int. Ed. Engl. 1994, 33, 1941.
22. (b) Herrmann, W. A.; Morawietz, M. J. A. J. Organomet. Chem. 1994, 482, 169.
23. (c) Herrmann, W. A.; Morawietz, M. J. A.; Priermeier, T.; Mashima, K. J. Organomet. Chem. 1995, 486, 291.
24. (d) Spence, R. E. v. H.; Piers, W. E. Organometallics 1995, 14, 4617.
25. (e) Scollard, J. D.; McConville, D. H.; Vittal, J. J. Organometallics 1995, 14, 5478.
26. Stevens, C. J.; Timmers, J. F.; Wilson, R. D.; Schmidt, G. F.; Nickias, P. N.; Rosen, R. K.; Knight, G. W.; Lai, S. Eur. Pat. Appl. 416 815, 1989.
27. Canich, J. A. M. U.S. Patent 5 026 798, 1990.
28. Jekel-Vroegop, C. T.; Teuben, J. H. J. Organomet. Chem. 1985, 286, 309.
29. (a) Bai, Y.; Roesky, H. W.; Noltemeyer, M. Z. Anorg. Allg. Chem. 1991, 595, 21.
30. (b) Bai, Y.; Noltemeyer, M.; Roesky, H. W. Z. Naturforsch. 1991, 46B, 1357.
31. Giolando, D. M.; Kirschbaum, K.; Graves, L. J.; Bolle, U. Inorg. Chem. 1992, 31, 3887.
32. (a) Martin, A.; Mena, M.; Yelamos, C.; Serrano, R.; Raithby, P. R. J. Organomet. Chem. 1994, 467, 79.
33. (b) Irigoyen, A. M.; Martin, A.; Mena, M.; Palacios, F.; Yelamos, C. J. Organomet. Chem. 1995, 494, 255.
34. Canich, J. A. M. WO 92/12162, 1992.
35. Herzog, A.; Liu, F.-Q.; Roesky, H. W.; Demsar, A.; Keller, K.; Noltemeyer, M.; Pauer, F. Organometallics 1994, 13, 1251.
36. Bai, Y.; Roesky, H. W.; Noltemeyer, M.; Witt, M. Chem. Ber. 1992, 125, 825.
37. Arney, D. J.; Bruck, M. A.; Huber, S. R.; Wigley, D. E. Inorg. Chem. 1992, 31, 3749.
38. Druce, P. M.; Kingston, B. M.; Lappert, M. F.; Srivastava, R. C.; Frazer, M. J.; Newton, W. E. J. Chem. Soc. A 1969, 2814.
39. The compound was found to crystallize in the triclinic space group P1 (a = 9.216(5) Å, b = 9.221(5) Å, c = 35.230(5) Å, α = 85.31(5)°, β = 78.87(5)°, γ = 61.22(4)°), with two independent molecules in the asymmetric unit.
40. (a) Herzog, A.; Roesky, H. W.; Zak, Z.; Noltemeyer, M. Angew. Chem. 1994, 106, 1035; Angew. Chem., Int. Ed. Engl. 1994, 33, 967.
41. (a) Herzog, A.; Roesky, H. W.; Zak, Z.; Noltemeyer, M. Angew. Chem. 1994, 106, 1035; Angew. Chem., Int. Ed. Engl. 1994, 33, 967.
42. (b) Shah, S. A. A.; Dorn, H.; Roesky, H. W. Unpublished results.
43. (a) Kaminsky, W.; Miri, M.; Sinn, H.; Woldt, R. Makromol. Chem. Rapid Commun. 1983, 4, 417.
44. (b) Kaminsky, W.; Külper, K.; Niedoba, S. Makromol. Chem., Makromol. Symp. 1986, 3, 377.
45. Chien, J. C. W.; Wang, B.-P. J. Polym. Sci. A: Polym. Chem. 1988, 26, 3089.
46. Ewen, J. A. J. Am. Chem. Soc. 1984, 106, 6355.
47. Heyn, B.; Hippler, B.; Kreisel, G.; Scheer, H.; Walther, D. Anorganische Synthesechemie; Springer-Verlag: Berlin, 1987.
48. Wolczanski, P. T.; Bercaw, J. E. Organometallics 1982, 1, 793.
49. Roddick, D. M.; Fryzuk, M. D.; Seidler, P. F.; Hillhouse, G. L.; Bercaw, J. E. Organometallics 1985, 4, 97.
50. Kennepohl, D. K.; Brooker, S.; Sheldrick, G. M.; Roesky, H. W. Chem. Ber. 1991, 124, 2223.
51. (a) Johnson, W. K. J. Org. Chem. 1960, 25, 2253.
52. (b) Levchuk, L. E.; Sams, J. R.; Aubke, F. Inorg. Chem. 1972, 11, 43.
53. (c) Krause, E. Ber. Dtsch. Chem. Ges. 1918, 51, 1447.
54. Clegg, W. Acta Crystallogr., Sect. A 1983, 39, 158.
55. Sheldrick, G. M. Acta Crystallogr., Sect. A 1990, 46, 467.
56. Sheldrick, G. M. SHELXL-93; University of Göttingen, Göttingen, Germany, 1993.