Simple enantiomeric excess determination of amines using chiral selones: † unusual N-H⋯Se bonding detected by HMQC 1H/77Se NMR spectroscopy

Chemical Communications

Volumn , Issue 10, 1996, Pages 1125-1126

  Wu, Ruilian ^a   Hernández, Griselda ^a   Odom, Jerome D ^b   Dunlap, R Bruce ^a,b   Silks, Louis A ^a  

^a LOS ALAMOS NATIONAL LABORATORY   (United States)

^b UNIVERSITY OF SOUTH CAROLINA   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000888966     PISSN: 13597345     EISSN: None     Source Type: Journal    
DOI: 10.1039/CC9960001125     Document Type: Article

References (19)

1. (a) S. C. Stinson, Chem. Eng. News, 1995, 73 (41), 44;
2. (b) D. Parker, Chem. Rev., 1991, 91, 1441;
3. (c) A. Alexakis, J. C. Frutos, S. Mutti and P. Mangeney, J. Org. Chem., 1994, 59, 3326.
4. (a) L. A. Silks, R. B. Dunlap and J. D. Odom, J. Am. Chem. Soc., 1990, 112, 4979;
5. (b) L. A. Silks, J. Peng, J. D. Odom and R. B. Dunlap, J. Chem. Soc. Perkins Trans I, 1991, 2495;
6. (c) L. A. Silks, J. Peng, R. B. Dunlap and J. D. Odom, J. Org. Chem., 1991, 56, 6733;
7. (d) J. Peng, M. E. Barr, D. A. Ashburn, J. D. Odom, R. B. Dunlap and L. A. Silks, J. Org. Chem., 1994, 59, 4977;
8. (e) J. Peng, D. A. Ashburn, M. E. Barr, L. Lebioda, R. A. Martinez, A. R. Garber, J. D. Odom, R. B. Dunlap and L. A. Silks, J. Org. Chem., 1995, 60, 5540;
9. (f) B. A. Salvatore and A. B. Smith III, Tetrahedron Lett., 1994, 35 (9), 1329;
10. (g) P. Michelsen, U. Annby and Gronowitz, S. Chem. Scr., 1984, 24, 251;
11. (h) H. Duddeck and T. Hotopp, Magn. Reson. Chem., 1995, 33, 490;
12. (i) H. Duddeck, Prog. Nucl. Magn. Reson. Spectrosc., 1995, 27, 1;
13. (j) R. Wu, J. D. Odom, R. B. Dunlap and L. A. Silk, Tetrahedron: Asymmetry, 1995, 6, 833.
14. L. A. Silks, J. Peng, J. D. Odom and R. B. Dunlap, Tetrahedron: Asymmetry, 1994, 5 (9), 1627.
15. M. Iwaoka and S. Tomosa, J. Am. Chem. Soc., 1994, 116, 4463.
16. J. O. Boles, W. H. Tolleson, J. C. Schmidt, R. B. Dunlap and J. D. Odom, J. Biol. Chem., 1992, 267, 22217; P. Gettins and B. C. Crews, J. Biol. Chem., 1991, 266, 4804; S. Muller, H. Senn, B. Gsell, W. Vetter, C. Baron and A. Böck, Biochemistry, 1994, 33, 3404.
17. J. O. Boles, W. H. Tolleson, J. C. Schmidt, R. B. Dunlap and J. D. Odom, J. Biol. Chem., 1992, 267, 22217; P. Gettins and B. C. Crews, J. Biol. Chem., 1991, 266, 4804; S. Muller, H. Senn, B. Gsell, W. Vetter, C. Baron and A. Böck, Biochemistry, 1994, 33, 3404.
18. J. O. Boles, W. H. Tolleson, J. C. Schmidt, R. B. Dunlap and J. D. Odom, J. Biol. Chem., 1992, 267, 22217; P. Gettins and B. C. Crews, J. Biol. Chem., 1991, 266, 4804; S. Muller, H. Senn, B. Gsell, W. Vetter, C. Baron and A. Böck, Biochemistry, 1994, 33, 3404.
19. A. Bax, R. H. Griffey and B. L. Hawkins, J. Magn. Reson., 1983, 55, 301.