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For reviews see: (a) Deacon, G. B.; Shen, Q. J. Organomet. Chem. 1996, 506, 1. (b) Edelmann, F. T. In Comprehensive Organometallic Chemistry; Abel, E. W., Stone, F. G. A., Wilkinson, G., Lappert, M. F., Eds; Pergamon: Oxford, England, 1995; Vol. 4, Chapter 2. (c) Schaverien, C. J. Adv. Oganomet. Chem. 1994, 36, 283. (d) Evans, W. J. Polyhedron 1987, 6, 803. (e) Watson, P. L.; Parshall, G. W. Acc Chem. Res. 1985, 15, 51. (f) Evans, W. J. Adv. Oganomet. Chem. 1985, 24, 131. (g) Schumann, H. Angew. Chem., Int. Ed. Engl. 1984, 23, 474. (h) Marks, T. J.; Ernst, R. D. In Comprehensive Organometallic Chemistry; Wilkinson, G., Stone, F. G. A., Abel, E. W., Eds; Pergamon: Oxford, England, 1982; Vol. 3, Chapter 21.
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For examples see: (a) Duchateau, R.; Meetsma, A.; Teuben, J. H. Organometallics 1996, 15, 1656. (b) Mashima, K.; Nakayama, Y.; Shibahara, T.; Fukumoto, H.; Nakamura, A. Inorg. Chem. 1996, 35, 93. (c) Evans, W. J.; Anwander, R.; Berlekamp, U. H.; Ziller, J. W. Inorg. Chem. 1995, 34, 3853. (d) van den Hende, J. R.; Hitchcock, P. B.; Holmes, S. A.; Lappert, M. F.; Leung, W.-P.; Mak, T. C. W.; Prashar, S. J. Chem. Soc. Dalton Trans. 1995, 1427. (e) Evans, W. J.; Anwander, R.; Ansari, M. A. ; Ziller, J. W. Inorg. Chem. 1995, 34, 5. (f) Schaverien, C. J. Organometallics 1994, 13, 69. (g) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Smith, J. D. J. Am. Chem. Soc. 1994, 116, 12071. (h) Hasinoff, L; Takats, J.; Zhang, X. W.; Bond, A. H.; Rogers, R. D. J. Am. Chem. Soc. 1994, 116, 8833. Maunder, G. H.; Sella, A.; Tocher, D. A. J. Chem. Soc., Chem. Commun. 1994, 2689. (j) Shapiro, P. J.; Cotter, W. D.; Schaefer, W. P.; Labinger, J. A.; Bercaw, J. E. J. Am. Chem. Soc. 1994, 116, 4623. (k) Sasai, H.; Arai, T.; Shibasaki, M. J. Am. Chem. Soc. 1994, 116, 1517. (l) Takats, J.; Zhang, X. W.; Day, V. W.; Eberspacher, T. A. Organometallics 1993, 12, 4286. (m) Bazan, G. C.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1993, 12, 2126. (n) Fryzuk, M. D.; Haddad, T. S.; Rettig, S. J. Organometallics 1992, 11, 2967.
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For examples see: (a) Duchateau, R.; Meetsma, A.; Teuben, J. H. Organometallics 1996, 15, 1656. (b) Mashima, K.; Nakayama, Y.; Shibahara, T.; Fukumoto, H.; Nakamura, A. Inorg. Chem. 1996, 35, 93. (c) Evans, W. J.; Anwander, R.; Berlekamp, U. H.; Ziller, J. W. Inorg. Chem. 1995, 34, 3853. (d) van den Hende, J. R.; Hitchcock, P. B.; Holmes, S. A.; Lappert, M. F.; Leung, W.-P.; Mak, T. C. W.; Prashar, S. J. Chem. Soc. Dalton Trans. 1995, 1427. (e) Evans, W. J.; Anwander, R.; Ansari, M. A. ; Ziller, J. W. Inorg. Chem. 1995, 34, 5. (f) Schaverien, C. J. Organometallics 1994, 13, 69. (g) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Smith, J. D. J. Am. Chem. Soc. 1994, 116, 12071. (h) Hasinoff, L; Takats, J.; Zhang, X. W.; Bond, A. H.; Rogers, R. D. J. Am. Chem. Soc. 1994, 116, 8833. Maunder, G. H.; Sella, A.; Tocher, D. A. J. Chem. Soc., Chem. Commun. 1994, 2689. (j) Shapiro, P. J.; Cotter, W. D.; Schaefer, W. P.; Labinger, J. A.; Bercaw, J. E. J. Am. Chem. Soc. 1994, 116, 4623. (k) Sasai, H.; Arai, T.; Shibasaki, M. J. Am. Chem. Soc. 1994, 116, 1517. (l) Takats, J.; Zhang, X. W.; Day, V. W.; Eberspacher, T. A. Organometallics 1993, 12, 4286. (m) Bazan, G. C.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1993, 12, 2126. (n) Fryzuk, M. D.; Haddad, T. S.; Rettig, S. J. Organometallics 1992, 11, 2967.
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For examples see: (a) Duchateau, R.; Meetsma, A.; Teuben, J. H. Organometallics 1996, 15, 1656. (b) Mashima, K.; Nakayama, Y.; Shibahara, T.; Fukumoto, H.; Nakamura, A. Inorg. Chem. 1996, 35, 93. (c) Evans, W. J.; Anwander, R.; Berlekamp, U. H.; Ziller, J. W. Inorg. Chem. 1995, 34, 3853. (d) van den Hende, J. R.; Hitchcock, P. B.; Holmes, S. A.; Lappert, M. F.; Leung, W.-P.; Mak, T. C. W.; Prashar, S. J. Chem. Soc. Dalton Trans. 1995, 1427. (e) Evans, W. J.; Anwander, R.; Ansari, M. A. ; Ziller, J. W. Inorg. Chem. 1995, 34, 5. (f) Schaverien, C. J. Organometallics 1994, 13, 69. (g) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Smith, J. D. J. Am. Chem. Soc. 1994, 116, 12071. (h) Hasinoff, L; Takats, J.; Zhang, X. W.; Bond, A. H.; Rogers, R. D. J. Am. Chem. Soc. 1994, 116, 8833. Maunder, G. H.; Sella, A.; Tocher, D. A. J. Chem. Soc., Chem. Commun. 1994, 2689. (j) Shapiro, P. J.; Cotter, W. D.; Schaefer, W. P.; Labinger, J. A.; Bercaw, J. E. J. Am. Chem. Soc. 1994, 116, 4623. (k) Sasai, H.; Arai, T.; Shibasaki, M. J. Am. Chem. Soc. 1994, 116, 1517. (l) Takats, J.; Zhang, X. W.; Day, V. W.; Eberspacher, T. A. Organometallics 1993, 12, 4286. (m) Bazan, G. C.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1993, 12, 2126. (n) Fryzuk, M. D.; Haddad, T. S.; Rettig, S. J. Organometallics 1992, 11, 2967.
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For examples see: (a) Duchateau, R.; Meetsma, A.; Teuben, J. H. Organometallics 1996, 15, 1656. (b) Mashima, K.; Nakayama, Y.; Shibahara, T.; Fukumoto, H.; Nakamura, A. Inorg. Chem. 1996, 35, 93. (c) Evans, W. J.; Anwander, R.; Berlekamp, U. H.; Ziller, J. W. Inorg. Chem. 1995, 34, 3853. (d) van den Hende, J. R.; Hitchcock, P. B.; Holmes, S. A.; Lappert, M. F.; Leung, W.-P.; Mak, T. C. W.; Prashar, S. J. Chem. Soc. Dalton Trans. 1995, 1427. (e) Evans, W. J.; Anwander, R.; Ansari, M. A. ; Ziller, J. W. Inorg. Chem. 1995, 34, 5. (f) Schaverien, C. J. Organometallics 1994, 13, 69. (g) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Smith, J. D. J. Am. Chem. Soc. 1994, 116, 12071. (h) Hasinoff, L; Takats, J.; Zhang, X. W.; Bond, A. H.; Rogers, R. D. J. Am. Chem. Soc. 1994, 116, 8833. Maunder, G. H.; Sella, A.; Tocher, D. A. J. Chem. Soc., Chem. Commun. 1994, 2689. (j) Shapiro, P. J.; Cotter, W. D.; Schaefer, W. P.; Labinger, J. A.; Bercaw, J. E. J. Am. Chem. Soc. 1994, 116, 4623. (k) Sasai, H.; Arai, T.; Shibasaki, M. J. Am. Chem. Soc. 1994, 116, 1517. (l) Takats, J.; Zhang, X. W.; Day, V. W.; Eberspacher, T. A. Organometallics 1993, 12, 4286. (m) Bazan, G. C.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1993, 12, 2126. (n) Fryzuk, M. D.; Haddad, T. S.; Rettig, S. J. Organometallics 1992, 11, 2967.
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For examples see: (a) Duchateau, R.; Meetsma, A.; Teuben, J. H. Organometallics 1996, 15, 1656. (b) Mashima, K.; Nakayama, Y.; Shibahara, T.; Fukumoto, H.; Nakamura, A. Inorg. Chem. 1996, 35, 93. (c) Evans, W. J.; Anwander, R.; Berlekamp, U. H.; Ziller, J. W. Inorg. Chem. 1995, 34, 3853. (d) van den Hende, J. R.; Hitchcock, P. B.; Holmes, S. A.; Lappert, M. F.; Leung, W.-P.; Mak, T. C. W.; Prashar, S. J. Chem. Soc. Dalton Trans. 1995, 1427. (e) Evans, W. J.; Anwander, R.; Ansari, M. A. ; Ziller, J. W. Inorg. Chem. 1995, 34, 5. (f) Schaverien, C. J. Organometallics 1994, 13, 69. (g) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Smith, J. D. J. Am. Chem. Soc. 1994, 116, 12071. (h) Hasinoff, L; Takats, J.; Zhang, X. W.; Bond, A. H.; Rogers, R. D. J. Am. Chem. Soc. 1994, 116, 8833. Maunder, G. H.; Sella, A.; Tocher, D. A. J. Chem. Soc., Chem. Commun. 1994, 2689. (j) Shapiro, P. J.; Cotter, W. D.; Schaefer, W. P.; Labinger, J. A.; Bercaw, J. E. J. Am. Chem. Soc. 1994, 116, 4623. (k) Sasai, H.; Arai, T.; Shibasaki, M. J. Am. Chem. Soc. 1994, 116, 1517. (l) Takats, J.; Zhang, X. W.; Day, V. W.; Eberspacher, T. A. Organometallics 1993, 12, 4286. (m) Bazan, G. C.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1993, 12, 2126. (n) Fryzuk, M. D.; Haddad, T. S.; Rettig, S. J. Organometallics 1992, 11, 2967.
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For examples see: (a) Duchateau, R.; Meetsma, A.; Teuben, J. H. Organometallics 1996, 15, 1656. (b) Mashima, K.; Nakayama, Y.; Shibahara, T.; Fukumoto, H.; Nakamura, A. Inorg. Chem. 1996, 35, 93. (c) Evans, W. J.; Anwander, R.; Berlekamp, U. H.; Ziller, J. W. Inorg. Chem. 1995, 34, 3853. (d) van den Hende, J. R.; Hitchcock, P. B.; Holmes, S. A.; Lappert, M. F.; Leung, W.-P.; Mak, T. C. W.; Prashar, S. J. Chem. Soc. Dalton Trans. 1995, 1427. (e) Evans, W. J.; Anwander, R.; Ansari, M. A. ; Ziller, J. W. Inorg. Chem. 1995, 34, 5. (f) Schaverien, C. J. Organometallics 1994, 13, 69. (g) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Smith, J. D. J. Am. Chem. Soc. 1994, 116, 12071. (h) Hasinoff, L; Takats, J.; Zhang, X. W.; Bond, A. H.; Rogers, R. D. J. Am. Chem. Soc. 1994, 116, 8833. Maunder, G. H.; Sella, A.; Tocher, D. A. J. Chem. Soc., Chem. Commun. 1994, 2689. (j) Shapiro, P. J.; Cotter, W. D.; Schaefer, W. P.; Labinger, J. A.; Bercaw, J. E. J. Am. Chem. Soc. 1994, 116, 4623. (k) Sasai, H.; Arai, T.; Shibasaki, M. J. Am. Chem. Soc. 1994, 116, 1517. (l) Takats, J.; Zhang, X. W.; Day, V. W.; Eberspacher, T. A. Organometallics 1993, 12, 4286. (m) Bazan, G. C.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1993, 12, 2126. (n) Fryzuk, M. D.; Haddad, T. S.; Rettig, S. J. Organometallics 1992, 11, 2967.
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For examples see: (a) Duchateau, R.; Meetsma, A.; Teuben, J. H. Organometallics 1996, 15, 1656. (b) Mashima, K.; Nakayama, Y.; Shibahara, T.; Fukumoto, H.; Nakamura, A. Inorg. Chem. 1996, 35, 93. (c) Evans, W. J.; Anwander, R.; Berlekamp, U. H.; Ziller, J. W. Inorg. Chem. 1995, 34, 3853. (d) van den Hende, J. R.; Hitchcock, P. B.; Holmes, S. A.; Lappert, M. F.; Leung, W.-P.; Mak, T. C. W.; Prashar, S. J. Chem. Soc. Dalton Trans. 1995, 1427. (e) Evans, W. J.; Anwander, R.; Ansari, M. A. ; Ziller, J. W. Inorg. Chem. 1995, 34, 5. (f) Schaverien, C. J. Organometallics 1994, 13, 69. (g) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Smith, J. D. J. Am. Chem. Soc. 1994, 116, 12071. (h) Hasinoff, L; Takats, J.; Zhang, X. W.; Bond, A. H.; Rogers, R. D. J. Am. Chem. Soc. 1994, 116, 8833. Maunder, G. H.; Sella, A.; Tocher, D. A. J. Chem. Soc., Chem. Commun. 1994, 2689. (j) Shapiro, P. J.; Cotter, W. D.; Schaefer, W. P.; Labinger, J. A.; Bercaw, J. E. J. Am. Chem. Soc. 1994, 116, 4623. (k) Sasai, H.; Arai, T.; Shibasaki, M. J. Am. Chem. Soc. 1994, 116, 1517. (l) Takats, J.; Zhang, X. W.; Day, V. W.; Eberspacher, T. A. Organometallics 1993, 12, 4286. (m) Bazan, G. C.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1993, 12, 2126. (n) Fryzuk, M. D.; Haddad, T. S.; Rettig, S. J. Organometallics 1992, 11, 2967.
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For examples see: (a) Duchateau, R.; Meetsma, A.; Teuben, J. H. Organometallics 1996, 15, 1656. (b) Mashima, K.; Nakayama, Y.; Shibahara, T.; Fukumoto, H.; Nakamura, A. Inorg. Chem. 1996, 35, 93. (c) Evans, W. J.; Anwander, R.; Berlekamp, U. H.; Ziller, J. W. Inorg. Chem. 1995, 34, 3853. (d) van den Hende, J. R.; Hitchcock, P. B.; Holmes, S. A.; Lappert, M. F.; Leung, W.-P.; Mak, T. C. W.; Prashar, S. J. Chem. Soc. Dalton Trans. 1995, 1427. (e) Evans, W. J.; Anwander, R.; Ansari, M. A. ; Ziller, J. W. Inorg. Chem. 1995, 34, 5. (f) Schaverien, C. J. Organometallics 1994, 13, 69. (g) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Smith, J. D. J. Am. Chem. Soc. 1994, 116, 12071. (h) Hasinoff, L; Takats, J.; Zhang, X. W.; Bond, A. H.; Rogers, R. D. J. Am. Chem. Soc. 1994, 116, 8833. Maunder, G. H.; Sella, A.; Tocher, D. A. J. Chem. Soc., Chem. Commun. 1994, 2689. (j) Shapiro, P. J.; Cotter, W. D.; Schaefer, W. P.; Labinger, J. A.; Bercaw, J. E. J. Am. Chem. Soc. 1994, 116, 4623. (k) Sasai, H.; Arai, T.; Shibasaki, M. J. Am. Chem. Soc. 1994, 116, 1517. (l) Takats, J.; Zhang, X. W.; Day, V. W.; Eberspacher, T. A. Organometallics 1993, 12, 4286. (m) Bazan, G. C.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1993, 12, 2126. (n) Fryzuk, M. D.; Haddad, T. S.; Rettig, S. J. Organometallics 1992, 11, 2967.
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13 we obtained crystals of 1 from THF/toluene, and 1·THF from pure THF.
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2542592120
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note
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The structure of 1 was inappropriately described previously as the ArO ligands occupying the apical positions and the three THF ligands taking the equatorial positions. See ref 13.
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Evans, W. J.; Drummond, D. K.; Grate, J. W.; Zhang, H.; Atwood, J. L. J. Am. Chem. Soc. 1987, 109, 3928.
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(1987)
J. Am. Chem. Soc.
, vol.109
, pp. 3928
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Evans, W.J.1
Drummond, D.K.2
Grate, J.W.3
Zhang, H.4
Atwood, J.L.5
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