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Volumn 35, Issue 5, 1996, Pages 1223-1234

Synthetic, Structural, Spectroscopic, and Theoretical Studies of Structural Isomers of the Cluster Pt3(μ-PPh2)3Ph(PPh3)2. A Unique Example of Core Isomerism in Phosphine Phosphido-Rich Clusters

(8) Bender, Robert a Braunstein, Pierre a Bedien, Alain a Ellis, Paul D b Huggins, Beth b Harvey, Pierre D c Sappa, Enrico d Tiripicchio, Antonio e

a UNIVERSITÉ DE STRASBOURG (France)

b UNIVERSITY OF SOUTH CAROLINA (United States)

c UNIVERSITÉ DE SHERBROOKE (Canada)

d UNIVERSITY OF TURIN (Italy)

e UNIVERSITY OF PARMA (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000826492 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic951164x Document Type: Article

Times cited : (92)

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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
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- Fultz, W.C.¹ Rheingold, A.L.² Kreter, P.E.³ Meek, D.W.⁴

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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
- (1983) J. Chem. Soc., Dalton Trans. , pp. 2229
- Haines, R.J.¹ Steen, N.D.C.T.² English, R.B.³

17
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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
- (1983) Organometallics , vol.2 , pp. 470
- Joncs, R.A.¹ Wright, T.C.² Atwood, J.L.³ Hunter, W.E.⁴

18
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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
- (1983) Organometallics , vol.2 , pp. 1249
- McKennis, J.S.¹ Kyba, E.P.²

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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
- (1984) J. Am. Chem. Soc. , vol.706 , pp. 5934
- Rosenberg, S.¹ Whittle, R.R.² Geoffroy, G.L.³

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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
- (1984) Organometallics , vol.3 , pp. 1020
- Regragui, R.¹ Dixneuf, P.² Taylor, N.J.³ Carty, A.J.⁴

21
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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
- (1984) J. Chem. Soc., Chem. Commun. , pp. 653
- Yu, Y.F.¹ Gallucei, J.² Wojcicki, A.³

22
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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
- (1985) J. Chem. Soc., Chem. Commun. , pp. 247
- Horten, A.D.¹ Mays, M.J.² Raithby, P.R.³

23
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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
- (1985) Angew. Chem, Int. Ed. Engl. , vol.24 , pp. 203
- Fischer, E.O.¹ Filippou, A.C.² Alt, H.G.³ Thewalt, U.⁴

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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (q) Gelmini, L.; Stephan, D. W. Inorg. Chim. Acta 1986, 111, L17. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
- (1985) J. Am. Chem. Soc. , vol.107 , pp. 501
- Ritchey, J.M.¹ Zozulin, A.J.² Wrobleski, D.A.³ Ryan, R.R.⁴ Wasserman, H.J.⁵ Moody, D.C.⁶ Payne, R.T.⁷

25
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- (b) Natarajan, K.; Zsolnai, L.; Huttner, G. Ibid. 1981, 220, 36. (c) Keller, E.; Vahrenkamp, H. Chem. Ber. 1981, 114, 1111. (d) Carty, A. J. Pure Appl Chem. 1982, 54, 113. (e) Collman, J. P.; Rothrock, R. K.; Finke, R. G.; Moore, E. J.; Rose-Munch, F Inorg. Chem. 1982, 21, 146. (f) Fultz, W. C.; Rheingold, A. L.; Kreter, P. E.; Meek, D. W. Ibid. 1983, 22, 860. (g) Haines, R. J.; Steen, N. D. C. T.; English, R. B. J. Chem. Soc., Dalton Trans. 1983, 2229. (h) Joncs, R A.; Wright, T. C.; Atwood, J. L.; Hunter, W. E. Organometallics 1983, 2, 470. (i) McKennis, J. S.; Kyba, E. P. Ibid. 1983, 2, 1249. (j) Rosenberg, S.; Whittle, R. R.; Geoffroy, G. L. J. Am. Chem. Soc. 1984, 706, 5934. (k) Regragui, R.; Dixneuf, P.; Taylor, N. J.; Carty, A. J Organometallics 1984, 3, 1020. (1) Yu, Y. F.; Gallucei, J.; Wojcicki, A. J. Chem. Soc., Chem. Commun. 1984, 653. (m) Horten, A. D.; Mays, M. J.; Raithby, P. R. Ibid. 1985, 247. (n) Fischer, E. O.; Filippou, A. C.; Alt, H. G.; Thewalt, U. Angew. Chem, Int. Ed. Engl. 1985, 24, 203. (o) Ritchey, J. M.; Zozulin, A. J.; Wrobleski, D. A.; Ryan, R. R.; Wasserman, H. J.; Moody, D. C.; Payne, R. T. J. Am. Chem. Soc. 1985, 107, 501. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (p) Roddick, D. M.; Santarsiero, B. D.; Bercaw, J. E. Ibid. 1985, 107, 4670. (r) Baker, R. T.; Tulip, T. H.; Wreford, S. S. Inorg. Chem. 1985, 24, 1379. (s) Hay, P. J.; Ryan, R. R.; Salazar, K. V.; Wrobleski, D. A.; Sattelberger, A. P. J. Am. Chem. Soc. 1986, 108, 313, (t) Targos, T. S.; Geoffroy, G. L., Rheingold, A. L. J. Organomet. Chem. 1986, 299, 223. (u) Arif, A. M.; Jones, R. A.; Seeberger, M. H.; Whittlesey, B. R.; Wright, T. C. Inorg. Chem. 1986, 25, 3943.
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- Roddick, D.M.¹ Santarsiero, B.D.² Bercaw, J.E.³

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