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Volumn 2, Issue 23, 2000, Pages 3591-3594

Laser flash photolysis of diphenylsulfonyldiazomethane: Detection of the sulfene and a sulfene-pyridine ylide

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EID: 0000813754     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol006463r     Document Type: Article
Times cited : (12)

References (56)
  • 1
    • 0002044959 scopus 로고
    • Moss, R. A., Jones, M. J., Eds.; Wiley-Interscience: New York
    • Moss, R. A.; Jones, M. J. Carbenes; Moss, R. A., Jones, M. J., Eds.; Wiley-Interscience: New York, 1985; Vol. 3, p 45.
    • (1985) Carbenes , vol.3 , pp. 45
    • Moss, R.A.1    Jones, M.J.2
  • 6
    • 0003828015 scopus 로고
    • J. Wiley and Sons: New York
    • Tidwell, T. T. Ketenes; J. Wiley and Sons: New York, 1995.
    • (1995) Ketenes
    • Tidwell, T.T.1
  • 12
    • 0001369347 scopus 로고
    • Thompson, L. F., Willson, C. G., Bowden, M. J., Eds.; American Chemical Society: Washington
    • Willson, C. G. Organic Resist Materials, 2nd ed.; Thompson, L. F., Willson, C. G., Bowden, M. J., Eds.; American Chemical Society: Washington, 1994; p 139.
    • (1994) Organic Resist Materials, 2nd Ed. , pp. 139
    • Willson, C.G.1
  • 28
    • 33847086807 scopus 로고
    • For the laser flash photolysis work, a Lumonics EX-530 excimer laser (Xe/HCl, 308 nm, ∼6 ns pulse width, 50-100 mJ/pulse) was used for excitation. The system is controlled by a Power Macintosh computer running LabVIEW 4.1 software. A Tektronix 2440 digital oscilloscope captures the signal from the photomultiplier tube. Further details on a similar system have been provided elsewhere (Scaiano, J. C. J. Am. Chem. Soc. 1980, 102, 7747. Scaiano, J. C.; Tanner, M.; Weir, D. J. Am. Chem. Soc. 1985, 107, 4396). The optical densities of the samples were 0.2-0.3 at the laser wavelength. A flow system (a 7 x 7 mm Suprasil quartz flow cell, connected with a 100 mL reservoir with Teflon tubing) was used in order to ensure irradiation of a fresh portion of the sample by each laser shot.
    • (1980) J. Am. Chem. Soc. , vol.102 , pp. 7747
    • Scaiano, J.C.1
  • 29
    • 33845376872 scopus 로고
    • For the laser flash photolysis work, a Lumonics EX-530 excimer laser (Xe/HCl, 308 nm, ∼6 ns pulse width, 50-100 mJ/pulse) was used for excitation. The system is controlled by a Power Macintosh computer running LabVIEW 4.1 software. A Tektronix 2440 digital oscilloscope captures the signal from the photomultiplier tube. Further details on a similar system have been provided elsewhere (Scaiano, J. C. J. Am. Chem. Soc. 1980, 102, 7747. Scaiano, J. C.; Tanner, M.; Weir, D. J. Am. Chem. Soc. 1985, 107, 4396). The optical densities of the samples were 0.2-0.3 at the laser wavelength. A flow system (a 7 x 7 mm Suprasil quartz flow cell, connected with a 100 mL reservoir with Teflon tubing) was used in order to ensure irradiation of a fresh portion of the sample by each laser shot.
    • (1985) J. Am. Chem. Soc. , vol.107 , pp. 4396
    • Scaiano, J.C.1    Tanner, M.2    Weir, D.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.