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(a) There was a significant amount of off-gases throughout the addition and until the reaction was complete. These gases contain HCl, CO, and oxalyl chloride. They should be scrubbed with a caustic scrubber or dissolved in running water by using a nonmetallic aspirator. (b) The distillate contains oxalyl chloride which should be carefully quenched with an appropriate alcohol and neutralized prior to disposal.
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