Synthesis and Characterization of the First Neutral Zinc-Sulfur Cluster: Zn10S4(SEt)12L4

Inorganic Chemistry

Volumn 35, Issue 4, 1996, Pages 802-803

  Nyman, May D ^a   Hampden Smith, Mark J ^a   Duesler, Eileen N ^a  

^a UNIVERSITY OF NEW MEXICO   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000762086     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic951470a     Document Type: Article

References (26)

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21. 4 and shows that this is the only crystalline phase present.
22. -3, Δ/σ(max) = 0 005. SHELXL software was used for all computations (G. Sheldrick, Siemens XRD, Madison, WI)
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24. 12 and formation of colloidal zinc sulfide.
25. 3). Lutidine ligands are displaced by pyridine solvent, but are present in a 1:1 ratio with Zn-SEt and Zn-Et. Anal. Calc. 36.7% C, 5.2% H, 3.89% N. Found: 34.2% C, 4.41% H, 3.17% N. We believe the elemental analysis data are low due to loss of lutidine.
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