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Volumn 43, Issue 12, 1996, Pages 2567-2593

Synthesis of dibenzo[d,f]-1,2-selena and -1,2-thiazepin-3-ones derivatives, bis-homoebselen

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EID: 0000735843     PISSN: 03855414     EISSN: None     Source Type: Journal    
DOI: 10.3987/com-96-7516     Document Type: Article
Times cited : (19)

References (37)
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    • 1H nmr (δ 7.10-7.90) and gave directly diselenide (25f) before complete characterization
    • 1H nmr (δ 7.10-7.90) and gave directly diselenide (25f) before complete characterization.
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    • Tlc analysis shows transformation of the cyclized product (4d) into unknown compound probably seleno sulfide (35) which disproportionates to diselenide (25f) and diphenyl disulfide (PhSSPh). GC-ms analysis confirms this result
    • Tlc analysis shows transformation of the cyclized product (4d) into unknown compound probably seleno sulfide (35) which disproportionates to diselenide (25f) and diphenyl disulfide (PhSSPh). GC-ms analysis confirms this result.


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