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Tetrahedron Letters
Volumn 26, Issue 3, 1985, Pages 359-362
2,6-Dimethylphenylnitrene in low-temperature matrices
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Indexed keywords

EID: 0000706584     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(01)80817-0     Document Type: Article
Times cited : (46)
References (11)
  • 3
    • 84918403973 scopus 로고    scopus 로고
    • T. Donnelly I.R. Dunkin D.S. Norwood A. Prentice C.J. Shields P.C.P. Thomson J. Chem. Soc. Perkin trans. 2, in press.
  • 7
    • 84918403972 scopus 로고    scopus 로고
    • Details of the cold cell have been published in detail previously (Ref. 8). The main features were a CsBr window enclosed in a vacuum-shroud and cooled by an Air Products Displex model CSA-202 helium refrigerator. Matrix gases were obtained from B.O.C. Ltd. (Research Grade), and the matrices were deposited by allowing the azide to sublime and condense on the cold window simultaneously with a large excess of the host gas. Matrix ratios could not be determined. Photolysis was carried out using an Oriel 200 W high pressure Hg arc, fitted with a quartz-windowed water-filter (λ ⪢ 200 nm). Pyrex (λ ⪢ 300 nm) and soda-glass (λ ⪢ 330 nm) filters were used as necessary. I.r. spectra were recorded on a Perkin Elmer model 684 spectrometer, interfaced with a Perkin Elmer model 3600 Data Station.
  • 8
    • 84918403971 scopus 로고    scopus 로고
    • I.R. Dunkin and J.G. MacDonald, J. Chem Soc., Perkin Trans. 2, in press
  • 11
    • 84918403970 scopus 로고    scopus 로고
    • G.A. Bell and I.R. Dunkin to be published.

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.