Niobium and tantalum diphosphanato complexes: Synthesis, structure, and NMR studies of Cp2MH[(PR)2] (R = Ph, Cy, H)

Organometallics

Volumn 16, Issue 15, 1997, Pages 3504-3510

  Etkin, Nola ^a   Benson, Michael T ^a,c   Courtenay, Silke ^a   McGlinchey, Michael J ^b   Bain, Alex D ^b   Stephan, Douglas W ^a  

^a UNIVERSITY OF WINDSOR   (Canada)

^b MCMASTER UNIVERSITY   (Canada)

^c University of Memphis   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000698078     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om970189w     Document Type: Article

References (23)

1. Ho, J.; Breen, T. L.; Ozarowski, A.; Stephan, D. W. Inorg. Chem. 1994, 33, 865.
2. Hou, Z.; Breen, T. L.; Stephan, D. W. Organometallics 1993, 12, 3158.
3. Fermin, M. C.; Stephan, D. W. J. Am. Chem. Soc. 1995, 117, 12645.
4. Etkin, N.; Fermin, M. C.; Stephan, D. W. J. Am. Chem. Soc. 1997, 119, in press.
5. Isseib, K.; Wille, G.; Krech, F. Angew. Chem., Int. Ed. Engl. 1972, 11, 527.
6. Benac, B. L.; Jones, R. A. Polyhedron 1989, 8, 1774.
7. (a) Hey-Hawkins, E. Z. Naturforsch. 1988, 43B, 1271.
8. (b) Fromm, K.; Baum, G.; Hey-Hawkins, E. Z. Anorg. Allg. Chem. 1992, 615, 35.
9. (a) Etkin, N.; Stephan, D. W. Unpublished results,
10. 2 with primary phosphines have been described: Vaughan, G. A.; Mulhouse, G.L.; Rheingold, A. L. Organometallics 1989, 8, 1760.
11. Leblanc, J. C.; Moise, C. J. Organomet. Chem. 1989, 364, C3.
12. (a) Nikonov, G. I. Lemenovskii, D. A.; Lorberth, J. Organometallics 1994, 13, 3127.
13. (b) Nikonov, G. I.; Kuzmina, L. G.; Mountford, P.; Lemenovskii, D. A. Organometallics 1995, 14, 3588.
14. Allman, T.; Bain, A. D.; Garbow, J. R. J. Magn. Reson. 1996, 123A, 26.
15. (a) Antinolo, A.; Chaudret, B.; Commenges, G.; Fajardo, M.; Jalon, F.; Morris, R. H.; Otero, A.; Schweitzer, C. T. J. Chem. Soc., Chem. Commun. 1988, 1210.
16. (b) Green, M. L. H.; Moreau, J. J. E. J. Organomet. Chem. 1978, 161, C25.
17. Schrock, R. R.; Sharp, P. R. J. Am. Chem. Soc. 1978, 100, 2389.
18. CaChe Worksystem Software is an integrated modeling, molecular mechanics, and molecular orbital computational software package and is a product of CaChe Scientific Inc.
19. (a) Cromer, D. T.; Mann, J. B. Acta Crystallogr. Sect. A: Cryst. Phys., Theor. Gen. Crystallogr. 1968, A24, 324.
20. (b) Cromer, D. T.; Mann, J. B. Acta Crystallogr. Sect. A: Cryst. Phys., Theor. Gen. Crystallogr. 1968, A24, 390.
21. Cromer, D. T.; Waber, J. T. International Tables for X-ray Crystallography; Knoch Press: Birmingham, England, 1974.
22. (a) Green, J. C.; Green, M. L. H.; Morris, G. E.; J. Chem. Soc., Chem Commun. 1974, 212.
23. (b) Cannillo, E.; Coda, A.; Prout, K.; Daran, J C. Acta Crystallogr. B. 1977, 33, 2608.