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85086289458
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note
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6) δ 91.62, 124.01, 138.48, 151.16, 168.27,
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25
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85086290206
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note
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2: C, 32.67; H, 1.46; N, 7.62. Found: C, 32.75; H, 1.50; N, 7.17.
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26
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85086288476
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note
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3) δ 2.98 (s, 1H), 4.91 (s, 1H), 6.75 (d, J = 7.1 Hz, 1H), 6.88 (s, 1H), 6.99 (d, J = 8.0 Hz, 1H), 7.12 (t, J = 6.2 Hz, 1H); MS m/z 119.
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27
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4243126839
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0342987551
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29
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4243119434
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note
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2: C, 43.63; H, 2.07; N, 6.64. Found: C, 43.45; H, 2.55; N, 6.21.
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30
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0028312651
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0027839947
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4243172315
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note
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To increase the molecular weights, more vigorous polymerizations at higher temperature or with longer polymerization time compared to those in Table 1 were performed. In those conditions, insoluble products were obtained, probably due to the extended coupling of ethynyl groups to form diacetylene units.
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34
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3843127431
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85086290718
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note
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3.
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36
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0026908991
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