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Volumn 16, Issue 24, 1997, Pages 5171-5182

Reactivity of cyclomanganated 2-phenylpyridine derivatives toward organolithium reagents. Synthesis of novel chelated tricarbonyl(η3-benzyl)manganese(I) complexes

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EID: 0000661614     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om970629j     Document Type: Article
Times cited : (37)

References (76)
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    • However, orthomangated triphenyl phosphite has been reported to undergo the insertion of alkynes: Grigsby, W. J.; Main, L.; Nicholson, B. K. Organometallics 1993, 12, 397.
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    • note
    • -.
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    • note
    • We observed that activated silica could induce a significant decomposition of the new complexes.
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    • 3-benzyl complexes are known to possess a fluxional behavior which is related to the weakness of the bond between the two aromatic carbons and the metal center. Please refer to references herein and to the following: (a) Brookhart, M.; Buck, R. C.; Danielson, E. J. Am. Chem. Soc. 1984, 111, 567. (b) Stühler, H. O. Angew. Chem. 1980, 92, 475. (c) Crascall, L. E.; Spencer, J. L. J. Chem. Soc., Dalton Trans. 1992, 3445. (d) Young, K. M.; Wrighton, M. S. J. Am. Chem. Soc. 1990, 112, 157.
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    • 3-benzyl complexes are known to possess a fluxional behavior which is related to the weakness of the bond between the two aromatic carbons and the metal center. Please refer to references herein and to the following: (a) Brookhart, M.; Buck, R. C.; Danielson, E. J. Am. Chem. Soc. 1984, 111, 567. (b) Stühler, H. O. Angew. Chem. 1980, 92, 475. (c) Crascall, L. E.; Spencer, J. L. J. Chem. Soc., Dalton Trans. 1992, 3445. (d) Young, K. M.; Wrighton, M. S. J. Am. Chem. Soc. 1990, 112, 157.
    • (1980) Angew. Chem. , vol.92 , pp. 475
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    • 3-benzyl complexes are known to possess a fluxional behavior which is related to the weakness of the bond between the two aromatic carbons and the metal center. Please refer to references herein and to the following: (a) Brookhart, M.; Buck, R. C.; Danielson, E. J. Am. Chem. Soc. 1984, 111, 567. (b) Stühler, H. O. Angew. Chem. 1980, 92, 475. (c) Crascall, L. E.; Spencer, J. L. J. Chem. Soc., Dalton Trans. 1992, 3445. (d) Young, K. M.; Wrighton, M. S. J. Am. Chem. Soc. 1990, 112, 157.
    • (1992) J. Chem. Soc., Dalton Trans. , pp. 3445
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    • 3-benzyl complexes are known to possess a fluxional behavior which is related to the weakness of the bond between the two aromatic carbons and the metal center. Please refer to references herein and to the following: (a) Brookhart, M.; Buck, R. C.; Danielson, E. J. Am. Chem. Soc. 1984, 111, 567. (b) Stühler, H. O. Angew. Chem. 1980, 92, 475. (c) Crascall, L. E.; Spencer, J. L. J. Chem. Soc., Dalton Trans. 1992, 3445. (d) Young, K. M.; Wrighton, M. S. J. Am. Chem. Soc. 1990, 112, 157.
    • (1990) J. Am. Chem. Soc. , vol.112 , pp. 157
    • Young, K.M.1    Wrighton, M.S.2
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    • (b) For a similar alternating bond length in 1,3-cycloheptadiene, see: Chiang, J. F.; Bauer, S. H. J. Am. Chem. Soc. 1966, 88, 420.
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    • A similar NMR dynamic effect has been reported for a strained (porphyrinato)osmium(II) ylide; Djukic, J. P.; Young, V. G.; Woo, L. K. Organometallics 1994, 13, 3995.
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